C₄₂H₆₀O₁₅

Base Information

Chemical Name:C₄₂H₆₀O₁₅
CAS No.:1351619-51-6
Molecular Formula:C₄₂H₆₀O₁₅
Molecular Weight:804.929
Hs Code.:

C<sub>42</sub>H<sub>60</sub>O<sub>15</sub>

Synonyms:C₄₂H₆₀O₁₅

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Chemical Property of C₄₂H₆₀O₁₅

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Technology Process of C₄₂H₆₀O₁₅

There total 12 articles about C₄₂H₆₀O₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1351619-46-9
C₄₂H₆₀O₁₄

: 1351619-51-6
C₄₂H₆₀O₁₅

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In acetonitrile; at 20 ℃; for 7h;
DOI:10.1016/j.tet.2011.09.058

Reference yield:

: 1351619-40-3
C₂₂H₂₉BrO₇

: 1351619-51-6
C₄₂H₆₀O₁₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: RuBr₂{(R)-2,2'-bis(diphenylphosphino)-1,1'-dinaphthyl}; hydrogen / ethanol / 44 h / 45 °C / 30003 Torr / High-pressure bomb

2.1: lithium triethylborohydride / tetrahydrofuran / 0 - 20 °C

3.1: 2,6-dimethylpyridine / dichloromethane / 22 h / 0 - 20 °C / Inert atmosphere

3.2: 2 h

4.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 6 h / 20 °C / Inert atmosphere

4.2: 1.5 h / 20 °C / Inert atmosphere

5.1: pyridine hydrogenfluoride / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere

6.1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; cesium fluoride / 1,4-dioxane / 2 h / 60 °C / Inert atmosphere

7.1: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water / 0.25 h / 20 °C

8.1: 3-chloro-benzenecarboperoxoic acid / acetonitrile / 7 h / 20 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; RuBr₂{(R)-2,2'-bis(diphenylphosphino)-1,1'-dinaphthyl}; 2,4,6-trichlorobenzoyl chloride; hydrogen; palladium diacetate; lithium triethylborohydride; pyridine hydrogenfluoride; triethylamine; 3-chloro-benzenecarboperoxoic acid; cesium fluoride; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; toluene; acetonitrile; 6.1: Suzuki coupling / 8.1: Baeyer-Villiger oxidation;
DOI:10.1016/j.tet.2011.09.058

Reference yield:

: 1351619-54-9
C₁₉H₂₅BrO₄

: 1351619-51-6
C₄₂H₆₀O₁₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: oxygen; ozone / dichloromethane / 0.07 h / -78 °C

1.2: 3 h / -78 - 20 °C

1.3: -78 - 20 °C

2.1: RuBr₂{(R)-2,2'-bis(diphenylphosphino)-1,1'-dinaphthyl}; hydrogen / ethanol / 44 h / 45 °C / 30003 Torr / High-pressure bomb

3.1: lithium triethylborohydride / tetrahydrofuran / 0 - 20 °C

4.1: 2,6-dimethylpyridine / dichloromethane / 22 h / 0 - 20 °C / Inert atmosphere

4.2: 2 h

5.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 6 h / 20 °C / Inert atmosphere

5.2: 1.5 h / 20 °C / Inert atmosphere

6.1: pyridine hydrogenfluoride / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere

7.1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; cesium fluoride / 1,4-dioxane / 2 h / 60 °C / Inert atmosphere

8.1: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water / 0.25 h / 20 °C

9.1: 3-chloro-benzenecarboperoxoic acid / acetonitrile / 7 h / 20 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; RuBr₂{(R)-2,2'-bis(diphenylphosphino)-1,1'-dinaphthyl}; 2,4,6-trichlorobenzoyl chloride; hydrogen; oxygen; palladium diacetate; lithium triethylborohydride; pyridine hydrogenfluoride; ozone; triethylamine; 3-chloro-benzenecarboperoxoic acid; cesium fluoride; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; toluene; acetonitrile; 1.3: Roskamp rearrangement / 7.1: Suzuki coupling / 9.1: Baeyer-Villiger oxidation;
DOI:10.1016/j.tet.2011.09.058