(3S,5S,6R,7aS)-3-(1,3-benzodioxol-5-yl)-5-benzyloxy-1-[(4-methylphenyl)sulfonyl]-2,3,5,6,7,7a-hexahydro-1H-6-indolol

Base Information

Chemical Name:(3S,5S,6R,7aS)-3-(1,3-benzodioxol-5-yl)-5-benzyloxy-1-[(4-methylphenyl)sulfonyl]-2,3,5,6,7,7a-hexahydro-1H-6-indolol
CAS No.:1067236-41-2
Molecular Formula:C₂₉H₂₉NO₆S
Molecular Weight:519.618
Hs Code.:

Synonyms:(3S,5S,6R,7aS)-3-(1,3-benzodioxol-5-yl)-5-benzyloxy-1-[(4-methylphenyl)sulfonyl]-2,3,5,6,7,7a-hexahydro-1H-6-indolol

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Chemical Property of (3S,5S,6R,7aS)-3-(1,3-benzodioxol-5-yl)-5-benzyloxy-1-[(4-methylphenyl)sulfonyl]-2,3,5,6,7,7a-hexahydro-1H-6-indolol

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Technology Process of (3S,5S,6R,7aS)-3-(1,3-benzodioxol-5-yl)-5-benzyloxy-1-[(4-methylphenyl)sulfonyl]-2,3,5,6,7,7a-hexahydro-1H-6-indolol

There total 1 articles about (3S,5S,6R,7aS)-3-(1,3-benzodioxol-5-yl)-5-benzyloxy-1-[(4-methylphenyl)sulfonyl]-2,3,5,6,7,7a-hexahydro-1H-6-indolol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1067236-40-1
(3S,5S,6R,7aS)-3-(1,3-benzodioxol-5-yl)-1-[(4-methylphenyl)sulfonyl]-2,3,5,6,7,7a-hexahydro-1H-indole-5,6-diol

: 1125-88-8
benzaldehyde dimethyl acetal

: 1067236-41-2
(3S,5S,6R,7aS)-3-(1,3-benzodioxol-5-yl)-5-benzyloxy-1-[(4-methylphenyl)sulfonyl]-2,3,5,6,7,7a-hexahydro-1H-6-indolol

Guidance literature:: (3S,5S,6R,7aS)-3-(1,3-benzodioxol-5-yl)-1-[(4-methylphenyl)sulfonyl]-2,3,5,6,7,7a-hexahydro-1H-indole-5,6-diol; benzaldehyde dimethyl acetal; With camphor-10-sulfonic acid; In dichloromethane; at 20 ℃; for 1h;

With diisobutylaluminium hydride; In dichloromethane; toluene; at -78 - 20 ℃; for 2h; Further stages.;
DOI:10.1021/jo801089y