(+/-)-(E)-1-<2-methyl-2-<(trimethylsilyl)oxy>-2-phenylacetoxy>-1,3-butadiene

Base Information

Chemical Name:(+/-)-(E)-1-<2-methyl-2-<(trimethylsilyl)oxy>-2-phenylacetoxy>-1,3-butadiene
CAS No.:136097-48-8
Molecular Formula:C₁₆H₂₂O₃Si
Molecular Weight:290.434
Hs Code.:

Synonyms:(+/-)-(E)-1-<2-methyl-2-<(trimethylsilyl)oxy>-2-phenylacetoxy>-1,3-butadiene

Suppliers and Price of (+/-)-(E)-1-<2-methyl-2-<(trimethylsilyl)oxy>-2-phenylacetoxy>-1,3-butadiene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-(E)-1-<2-methyl-2-<(trimethylsilyl)oxy>-2-phenylacetoxy>-1,3-butadiene

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Technology Process of (+/-)-(E)-1-<2-methyl-2-<(trimethylsilyl)oxy>-2-phenylacetoxy>-1,3-butadiene

There total 1 articles about (+/-)-(E)-1-<2-methyl-2-<(trimethylsilyl)oxy>-2-phenylacetoxy>-1,3-butadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 136066-60-9
(+/-)-3-<2-methyl-2-<(trimethylsilyl)oxo>-2-phenylacetoxy>-endo-tricyclo<4.2.1.0^2,5>non-7-ene

: 136097-48-8
(+/-)-(E)-1-<2-methyl-2-<(trimethylsilyl)oxy>-2-phenylacetoxy>-1,3-butadiene

Guidance literature:: at 25 - 250 ℃;
DOI:10.1021/ja00020a026

Reference yield:

: 128-53-0
N-Ethylmaleimide

: 136097-48-8
(+/-)-(E)-1-<2-methyl-2-<(trimethylsilyl)oxy>-2-phenylacetoxy>-1,3-butadiene

: 136066-53-0,136066-55-2
(S)-2-Phenyl-2-trimethylsilanyloxy-propionic acid (3aS,4R,7aS)-2-ethyl-1,3-dioxo-2,3,3a,4,7,7a-hexahydro-1H-isoindol-4-yl ester

: 136066-53-0,136066-55-2
(R)-2-Phenyl-2-trimethylsilanyloxy-propionic acid (3aS,4R,7aS)-2-ethyl-1,3-dioxo-2,3,3a,4,7,7a-hexahydro-1H-isoindol-4-yl ester

Guidance literature:: In toluene; at 25 ℃; Title compound not separated from byproducts;
DOI:10.1021/ja00020a026

Reference yield:

: 128-53-0
N-Ethylmaleimide

: 136097-48-8
(+/-)-(E)-1-<2-methyl-2-<(trimethylsilyl)oxy>-2-phenylacetoxy>-1,3-butadiene

: 136066-52-9,136066-54-1
(R)-2-Hydroxy-2-phenyl-propionic acid (3aR,4S,7aR)-2-ethyl-1,3-dioxo-2,3,3a,4,7,7a-hexahydro-1H-isoindol-4-yl ester

: 136066-52-9,136066-54-1
(S)-2-Hydroxy-2-phenyl-propionic acid (3aR,4S,7aR)-2-ethyl-1,3-dioxo-2,3,3a,4,7,7a-hexahydro-1H-isoindol-4-yl ester

Guidance literature:: With oxalic acid; Yield given. Multistep reaction; 1.) toluene, 25 deg C, 2.) MeOH, 25 deg C, 1 h;
DOI:10.1021/ja00020a026