Technology Process of C19H28O2
There total 5 articles about C19H28O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C18H28O3;
With
sodium hydride;
In
tetrahydrofuran; mineral oil;
at 0 - 20 ℃;
for 1h;
With
1-[(2,4,6-triisopropylphenyl)sulfonyl]-1H-imidazole;
In
tetrahydrofuran; mineral oil;
at 0 - 20 ℃;
for 2h;
DOI:10.1021/ol1028699
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: ammonium molibdate; dihydrogen peroxide / ethanol / 21 h / 0 °C
2.1: sodium hexamethyldisilazane / 1,2-dimethoxyethane; toluene / 0.08 h / -78 °C
2.2: 1 h / -50 °C
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 0 - 20 °C
4.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C
4.2: 2 h / 0 - 20 °C
With
ammonium molibdate; tetrabutyl ammonium fluoride; dihydrogen peroxide; sodium hexamethyldisilazane; sodium hydride;
In
tetrahydrofuran; 1,2-dimethoxyethane; ethanol; toluene; mineral oil;
2.1: Julia Olefin synthesis / 2.2: Julia Olefin synthesis;
DOI:10.1021/ol1028699
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hexamethyldisilazane / 1,2-dimethoxyethane; toluene / 0.08 h / -78 °C
1.2: 1 h / -50 °C
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 0 - 20 °C
3.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C
3.2: 2 h / 0 - 20 °C
With
tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; sodium hydride;
In
tetrahydrofuran; 1,2-dimethoxyethane; toluene; mineral oil;
1.1: Julia Olefin synthesis / 1.2: Julia Olefin synthesis;
DOI:10.1021/ol1028699
