25-[4-(5-phenyl-1H-pyrrol-3-yl)-benzyl]-1,4,7,10,13,16,19,22-octaoxa-25-aza-cycloheptacosane

Base Information

Chemical Name:25-[4-(5-phenyl-1H-pyrrol-3-yl)-benzyl]-1,4,7,10,13,16,19,22-octaoxa-25-aza-cycloheptacosane
CAS No.:934161-05-4
Molecular Formula:C₃₅H₅₀N₂O₈
Molecular Weight:626.791
Hs Code.:

25-[4-(5-phenyl-1<i>H</i>-pyrrol-3-yl)-benzyl]-1,4,7,10,13,16,19,22-octaoxa-25-aza-cycloheptacosane

Synonyms:25-[4-(5-phenyl-1H-pyrrol-3-yl)-benzyl]-1,4,7,10,13,16,19,22-octaoxa-25-aza-cycloheptacosane

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Chemical Property of 25-[4-(5-phenyl-1H-pyrrol-3-yl)-benzyl]-1,4,7,10,13,16,19,22-octaoxa-25-aza-cycloheptacosane

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Technology Process of 25-[4-(5-phenyl-1H-pyrrol-3-yl)-benzyl]-1,4,7,10,13,16,19,22-octaoxa-25-aza-cycloheptacosane

There total 5 articles about 25-[4-(5-phenyl-1H-pyrrol-3-yl)-benzyl]-1,4,7,10,13,16,19,22-octaoxa-25-aza-cycloheptacosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 934161-03-2
4-nitro-3-[4-(1,4,7,10,13,16,19,22-octaoxa-25-aza-cycloheptacos-25-ylmethyl)-phenyl]-1-phenyl-butan-1-one

: 934161-05-4
25-[4-(5-phenyl-1H-pyrrol-3-yl)-benzyl]-1,4,7,10,13,16,19,22-octaoxa-25-aza-cycloheptacosane

Guidance literature:: 4-nitro-3-[4-(1,4,7,10,13,16,19,22-octaoxa-25-aza-cycloheptacos-25-ylmethyl)-phenyl]-1-phenyl-butan-1-one; With potassium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 1h;

With sulfuric acid; In tetrahydrofuran; methanol; at 0 - 20 ℃;

With ammonium acetate; acetic acid; at 110 ℃; for 1.5h;
DOI:10.1021/jo062506r

Reference yield:

: 934160-99-3
4-(1,4,7,10,13,16,19,22-octaoxa-25-aza-cycloheptacos-25-ylmethyl)-benzaldehyde

: 934161-05-4
25-[4-(5-phenyl-1H-pyrrol-3-yl)-benzyl]-1,4,7,10,13,16,19,22-octaoxa-25-aza-cycloheptacosane

Guidance literature:: Multi-step reaction with 3 steps

1.1: 90 percent / NaOH / methanol / 15 h / 20 °C

2.1: 95 percent / Et₂NH / methanol / 17 h / 75 °C

3.1: KOH / methanol; tetrahydrofuran / 1 h / 20 °C

3.2: H₂SO₄ / methanol; tetrahydrofuran / 0 - 20 °C

3.3: 49 percent / NH₄OAc; AcOH / 1.5 h / 110 °C

With potassium hydroxide; sodium hydroxide; diethylamine; In tetrahydrofuran; methanol; 2.1: Henry addition / 3.1: Nef reaction;
DOI:10.1021/jo062506r

Reference yield:

: 934161-01-0
3-[4-(1,4,7,10,13,16,19,22-octaoxa-25-aza-cycloheptacos-25-ylmethyl)-phenyl]-1-phenyl-propenone

: 934161-05-4
25-[4-(5-phenyl-1H-pyrrol-3-yl)-benzyl]-1,4,7,10,13,16,19,22-octaoxa-25-aza-cycloheptacosane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 95 percent / Et₂NH / methanol / 17 h / 75 °C

2.1: KOH / methanol; tetrahydrofuran / 1 h / 20 °C

2.2: H₂SO₄ / methanol; tetrahydrofuran / 0 - 20 °C

2.3: 49 percent / NH₄OAc; AcOH / 1.5 h / 110 °C

With potassium hydroxide; diethylamine; In tetrahydrofuran; methanol; 1.1: Henry addition / 2.1: Nef reaction;
DOI:10.1021/jo062506r