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Technology Process of trans,trans-(C6F5)((p-C6H4-t-Bu)2P-(CH2)14P(p-C6H4-t-Bu)2Pt-(C2)4Pt-((p-C6H4-t-Bu)2P(CH2)14P-(p-C6H4-t-Bu)2)(C6F5)

trans,trans-(C6F5)((p-C6H4-t-Bu)2P-(CH2)14P(p-C6H4-t-Bu)2Pt-(C2)4Pt-((p-C6H4-t-Bu)2P(CH2)14P-(p-C6H4-t-Bu)2)(C6F5)

Base Information
  • Chemical Name:trans,trans-(C6F5)((p-C6H4-t-Bu)2P-(CH2)14P(p-C6H4-t-Bu)2Pt-(C2)4Pt-((p-C6H4-t-Bu)2P(CH2)14P-(p-C6H4-t-Bu)2)(C6F5)
  • CAS No.:464896-30-8
  • Molecular Formula:C128H160F10P4Pt2
  • Molecular Weight:2402.72
  • Hs Code.:
trans,trans-(C<sub>6</sub>F<sub>5</sub>)((p-C<sub>6</sub>H<sub>4</sub>-t-Bu)2P-(CH<sub>2</sub>)14P(p-C<sub>6</sub>H<sub>4</sub>-t-Bu)2Pt-(C<sub>2</sub>)4Pt-((p-C<sub>6</sub>H<sub>4</sub>-t-Bu)2P(CH<sub>2</sub>)14P-(p-C<sub>6</sub>H<sub>4</sub>-t-Bu)2)(C<sub>6</sub>F<sub>5</sub>)

Synonyms:trans,trans-(C6F5)((p-C6H4-t-Bu)2P-(CH2)14P(p-C6H4-t-Bu)2Pt-(C2)4Pt-((p-C6H4-t-Bu)2P(CH2)14P-(p-C6H4-t-Bu)2)(C6F5)

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Chemical Property of trans,trans-(C6F5)((p-C6H4-t-Bu)2P-(CH2)14P(p-C6H4-t-Bu)2Pt-(C2)4Pt-((p-C6H4-t-Bu)2P(CH2)14P-(p-C6H4-t-Bu)2)(C6F5)
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Technology Process of trans,trans-(C6F5)((p-C6H4-t-Bu)2P-(CH2)14P(p-C6H4-t-Bu)2Pt-(C2)4Pt-((p-C6H4-t-Bu)2P(CH2)14P-(p-C6H4-t-Bu)2)(C6F5)

There total 1 articles about trans,trans-(C6F5)((p-C6H4-t-Bu)2P-(CH2)14P(p-C6H4-t-Bu)2Pt-(C2)4Pt-((p-C6H4-t-Bu)2P(CH2)14P-(p-C6H4-t-Bu)2)(C6F5) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

((CH<sub>3</sub>)3CC<sub>6</sub>H<sub>4</sub>)2P(CH<sub>2</sub>)14P(C<sub>6</sub>H<sub>4</sub>C(CH<sub>3</sub>)3)2
464896-39-7

((CH3)3CC6H4)2P(CH2)14P(C6H4C(CH3)3)2

trans,trans-(C<sub>6</sub>F<sub>5</sub>)((p-tolyl)3P)2Pt(CC)4Pt(P(p-tolyl)3)2(C<sub>6</sub>F<sub>5</sub>)

trans,trans-(C6F5)((p-tolyl)3P)2Pt(CC)4Pt(P(p-tolyl)3)2(C6F5)

trans,trans-(C<sub>6</sub>F<sub>5</sub>)((p-C<sub>6</sub>H<sub>4</sub>-t-Bu)2P-(CH<sub>2</sub>)14P(p-C<sub>6</sub>H<sub>4</sub>-t-Bu)2Pt-(C<sub>2</sub>)4Pt-((p-C<sub>6</sub>H<sub>4</sub>-t-Bu)2P(CH<sub>2</sub>)14P-(p-C<sub>6</sub>H<sub>4</sub>-t-Bu)2)(C<sub>6</sub>F<sub>5</sub>)
464896-30-8

trans,trans-(C6F5)((p-C6H4-t-Bu)2P-(CH2)14P(p-C6H4-t-Bu)2Pt-(C2)4Pt-((p-C6H4-t-Bu)2P(CH2)14P-(p-C6H4-t-Bu)2)(C6F5)

Guidance literature:
In dichloromethane; a Schlenk flack was charged with Pt-complex and CH2Cl2, a soln. of diphosphine in CH2Cl2 was passed through a silica gel pad with stirring, 2 h of stirring; the solvent was removed by oil pump vac., ethanol was added, filtered, washed with ethanol, dried by oil pump vac.; elem. anal.;
DOI:10.1021/ja0716103
upstream raw materials:

((CH3)3CC6H4)2P(CH2)14P(C6H4C(CH3)3)2

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