2-amino-6-[(2-aminoethyl)sulfanyl]-4-(4-hydroxyphenyl)-3,5-pyridinedicarbonitrile

Base Information

Chemical Name:2-amino-6-[(2-aminoethyl)sulfanyl]-4-(4-hydroxyphenyl)-3,5-pyridinedicarbonitrile
CAS No.:333963-37-4
Molecular Formula:C₁₅H₁₃N₅OS
Molecular Weight:311.367
Hs Code.:

Synonyms:2-amino-6-[(2-aminoethyl)sulfanyl]-4-(4-hydroxyphenyl)-3,5-pyridinedicarbonitrile

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Chemical Property of 2-amino-6-[(2-aminoethyl)sulfanyl]-4-(4-hydroxyphenyl)-3,5-pyridinedicarbonitrile

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Technology Process of 2-amino-6-[(2-aminoethyl)sulfanyl]-4-(4-hydroxyphenyl)-3,5-pyridinedicarbonitrile

There total 1 articles about 2-amino-6-[(2-aminoethyl)sulfanyl]-4-(4-hydroxyphenyl)-3,5-pyridinedicarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.2%

: 2576-47-8
2-bromoethylamine hydrobromide

: 221178-83-2
2-amino-4-(4-hydroxyphenyl)-6-mercaptopyridine-3,5-dicarbonitrile

: 333963-37-4
2-amino-6-[(2-aminoethyl)sulfanyl]-4-(4-hydroxyphenyl)-3,5-pyridinedicarbonitrile

Guidance literature:: 2-bromoethylamine hydrobromide; 2-amino-4-(4-hydroxyphenyl)-6-mercaptopyridine-3,5-dicarbonitrile; With sodium hydrogencarbonate; In N,N-dimethyl-formamide; for 1h;

With hydrogenchloride; water; In N,N-dimethyl-formamide;

Reference yield: 62.3%

: 333963-37-4
2-amino-6-[(2-aminoethyl)sulfanyl]-4-(4-hydroxyphenyl)-3,5-pyridinedicarbonitrile

: 624-83-9
methyl isocyanate

: 333963-47-6
N-(2-{[6-amino-3,5-dicyano-4-(4-hydroxyphenyl)-2-pyridinyl]sulfanyl}ethyl)-N'-methylurea

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃;

Reference yield: 58.7%

: 333963-37-4
2-amino-6-[(2-aminoethyl)sulfanyl]-4-(4-hydroxyphenyl)-3,5-pyridinedicarbonitrile

: 79-22-1
methyl chloroformate

: 333963-41-0
(2-{[6-amino-3,5-dicyano-4-(4-hydroxyphenyl)-2-pyridinyl]sulfanyl}ethyl)-methylcarbamate

Guidance literature:: 2-amino-6-[(2-aminoethyl)sulfanyl]-4-(4-hydroxyphenyl)-3,5-pyridinedicarbonitrile; methyl chloroformate; With triethylamine; In dichloromethane; at -25 - 0 ℃; for 1.5h;

With methanol; ammonia; at 20 ℃; for 1h;