N-acetyl-2-(3-methylbutyn-1-yl)-5-carbomethoxyaniline

Base Information

Chemical Name:N-acetyl-2-(3-methylbutyn-1-yl)-5-carbomethoxyaniline
CAS No.:123028-06-8
Molecular Formula:C₁₅H₁₇NO₃
Molecular Weight:259.305
Hs Code.:

Synonyms:N-acetyl-2-(3-methylbutyn-1-yl)-5-carbomethoxyaniline

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Chemical Property of N-acetyl-2-(3-methylbutyn-1-yl)-5-carbomethoxyaniline

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Technology Process of N-acetyl-2-(3-methylbutyn-1-yl)-5-carbomethoxyaniline

There total 4 articles about N-acetyl-2-(3-methylbutyn-1-yl)-5-carbomethoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.1%

: 58064-11-2
Tributyl-(3-methylbut-1-ynyl)stannane

: 123027-98-5
N-acetyl-5-carbomethoxy-2-<(trifluoromethyl)sulfonyl>aniline

: 123028-06-8
N-acetyl-2-(3-methylbutyn-1-yl)-5-carbomethoxyaniline

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium chloride; In 1,4-dioxane; at 100 ℃; for 1.75h;
DOI:10.1021/jo00286a014

Reference yield:

: 17763-71-2
4-carbomethoxyphenyl triflate

: 123028-06-8
N-acetyl-2-(3-methylbutyn-1-yl)-5-carbomethoxyaniline

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / H₂SO₄, concd HNO₃ / 14 h / Ambient temperature

2: 83.8 percent / iron, acetic acid / ethanol / 2 h / Heating

3: 71.3 percent / pyridine / CH₂Cl₂ / 20 h / 23 °C

4: 77.1 percent / lithium chloride, tetrakis(triphenylphosphine)palladium / dioxane / 1.75 h / 100 °C

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; nitric acid; iron; acetic acid; lithium chloride; In 1,4-dioxane; ethanol; dichloromethane;
DOI:10.1021/jo00286a014

Reference yield:

: 123027-97-4
2-amino-4-carbomethoxyphenyl trifluoromethanesulfonate

: 123028-06-8
N-acetyl-2-(3-methylbutyn-1-yl)-5-carbomethoxyaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 71.3 percent / pyridine / CH₂Cl₂ / 20 h / 23 °C

2: 77.1 percent / lithium chloride, tetrakis(triphenylphosphine)palladium / dioxane / 1.75 h / 100 °C

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium chloride; In 1,4-dioxane; dichloromethane;
DOI:10.1021/jo00286a014