(S)-trimethyl(2-methylene-5-phenoxy-4-(trimethylsilyloxy)pentyl)silane

Base Information

Chemical Name:(S)-trimethyl(2-methylene-5-phenoxy-4-(trimethylsilyloxy)pentyl)silane
CAS No.:1177441-11-0
Molecular Formula:C₁₈H₃₂O₂Si₂
Molecular Weight:336.622
Hs Code.:

Synonyms:(S)-trimethyl(2-methylene-5-phenoxy-4-(trimethylsilyloxy)pentyl)silane

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Chemical Property of (S)-trimethyl(2-methylene-5-phenoxy-4-(trimethylsilyloxy)pentyl)silane

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Technology Process of (S)-trimethyl(2-methylene-5-phenoxy-4-(trimethylsilyloxy)pentyl)silane

There total 1 articles about (S)-trimethyl(2-methylene-5-phenoxy-4-(trimethylsilyloxy)pentyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 18297-63-7,127290-39-5
N,N'-bis(trimethylsilyl)urea

: 1177441-09-6
(S)-1-phenoxy-4-((trimethylsilyl)methyl)pent-4-en-2-ol

: 1177441-11-0
(S)-trimethyl(2-methylene-5-phenoxy-4-(trimethylsilyloxy)pentyl)silane

Guidance literature:: In tetrahydrofuran; at 80 ℃; for 16h;
DOI:10.1021/ol901201k

Reference yield: 84.0%

: 1177441-11-0
(S)-trimethyl(2-methylene-5-phenoxy-4-(trimethylsilyloxy)pentyl)silane

: 2403-59-0
p-(diethoxymethyl)toluene

: 1177441-13-2
(2S,6R)-4-methylene-2-(phenoxymethyl)-6-p-tolyltetrahydro-2H-pyran

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at -78 ℃; for 14h; optical yield given as %de; Molecular sieve;
DOI:10.1021/ol901201k

Reference yield: 80.0%

: 1670-47-9
1,1-diethoxycyclohexane

: 1177441-11-0
(S)-trimethyl(2-methylene-5-phenoxy-4-(trimethylsilyloxy)pentyl)silane

: 1177441-12-1
(S)-4-methylene-2-(phenoxymethyl)-1-oxaspiro[5.5]undecane

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at -78 ℃; for 5h; Molecular sieve;
DOI:10.1021/ol901201k