diethyl (S)-1-((R)-tert-butylsulfinamido)-2,2,2-trifluoro-1-p-tolylethylphosphonate

Base Information

Chemical Name:diethyl (S)-1-((R)-tert-butylsulfinamido)-2,2,2-trifluoro-1-p-tolylethylphosphonate
CAS No.:1472660-54-0
Molecular Formula:C₁₇H₂₇F₃NO₄PS
Molecular Weight:429.441
Hs Code.:

Synonyms:diethyl (S)-1-((R)-tert-butylsulfinamido)-2,2,2-trifluoro-1-p-tolylethylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl (S)-1-((R)-tert-butylsulfinamido)-2,2,2-trifluoro-1-p-tolylethylphosphonate

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Technology Process of diethyl (S)-1-((R)-tert-butylsulfinamido)-2,2,2-trifluoro-1-p-tolylethylphosphonate

There total 1 articles about diethyl (S)-1-((R)-tert-butylsulfinamido)-2,2,2-trifluoro-1-p-tolylethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 394-59-2
2,2,2-trifluoro-1-(p-tolyl)ethanone

: 762-04-9
phosphonic acid diethyl ester

: 196929-78-9
(R)-2-methylpropane-2-sulfinamide

: 1472660-54-0
diethyl (S)-1-((R)-tert-butylsulfinamido)-2,2,2-trifluoro-1-p-tolylethylphosphonate

: diethyl (R)-1-((R)-tert-butylsulfinamido)-2,2,2-trifluoro-1-p-tolylethylphosphonate

Guidance literature:: 2,2,2-trifluoro-1-(p-tolyl)ethanone; (R)-2-methylpropane-2-sulfinamide; With titanium(IV) isopropylate; In hexane; toluene; at 20 ℃; for 12h; Inert atmosphere;

phosphonic acid diethyl ester; In hexane; toluene; at -40 ℃; Overall yield = 65 %; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/cjoc.201300344