Benzoic acid (2R,5S)-5-(4-amino-2-oxo-2H-pyrimidin-1-yl)-[1,3]oxathiolan-2-ylmethyl ester

Base Information

Chemical Name:Benzoic acid (2R,5S)-5-(4-amino-2-oxo-2H-pyrimidin-1-yl)-[1,3]oxathiolan-2-ylmethyl ester
CAS No.:143957-12-4
Molecular Formula:C₁₅H₁₅N₃O₄S
Molecular Weight:333.368
Hs Code.:

Synonyms:Benzoic acid (2R,5S)-5-(4-amino-2-oxo-2H-pyrimidin-1-yl)-[1,3]oxathiolan-2-ylmethyl ester

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Chemical Property of Benzoic acid (2R,5S)-5-(4-amino-2-oxo-2H-pyrimidin-1-yl)-[1,3]oxathiolan-2-ylmethyl ester

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Technology Process of Benzoic acid (2R,5S)-5-(4-amino-2-oxo-2H-pyrimidin-1-yl)-[1,3]oxathiolan-2-ylmethyl ester

There total 4 articles about Benzoic acid (2R,5S)-5-(4-amino-2-oxo-2H-pyrimidin-1-yl)-[1,3]oxathiolan-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64904-47-8
2-benzoyloxyacetaldehyde

: 143957-12-4
Benzoic acid (2R,5S)-5-(4-amino-2-oxo-2H-pyrimidin-1-yl)-[1,3]oxathiolan-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride etherate / acetonitrile

2: 64 percent / dimethylformamide

3: iodotrimethylsilane (TMSI) / 1,2-dichloro-ethane

With trimethylsilyl iodide; boron trifluoride diethyl etherate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(00)61330-8

Reference yield:

: 143957-11-3
(2R,5S)-2-Benzoyloxymethyl-[1,3]oxathiolane-5-carboxylic acid

: 143957-12-4
Benzoic acid (2R,5S)-5-(4-amino-2-oxo-2H-pyrimidin-1-yl)-[1,3]oxathiolan-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / dimethylformamide

2: iodotrimethylsilane (TMSI) / 1,2-dichloro-ethane

With trimethylsilyl iodide; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)61330-8

Reference yield:

: 143919-90-8,143957-14-6,146726-76-3
((2R)-5-acetoxy-1,3-oxathiolan-2-yl)methyl benzoate

: 143957-12-4
Benzoic acid (2R,5S)-5-(4-amino-2-oxo-2H-pyrimidin-1-yl)-[1,3]oxathiolan-2-ylmethyl ester

Guidance literature:: With trimethylsilyl iodide; In 1,2-dichloro-ethane; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4039(00)61330-8