(1R,2S,3S,5S)-8-Methyl-3-p-tolyl-8-aza-bicyclo[3.2.1]octane-2-carbonyl chloride

Base Information

Chemical Name:(1R,2S,3S,5S)-8-Methyl-3-p-tolyl-8-aza-bicyclo[3.2.1]octane-2-carbonyl chloride
CAS No.:204071-17-0
Molecular Formula:C₁₆H₂₀ClNO
Molecular Weight:277.794
Hs Code.:

Synonyms:(1R,2S,3S,5S)-8-Methyl-3-p-tolyl-8-aza-bicyclo[3.2.1]octane-2-carbonyl chloride

Suppliers and Price of (1R,2S,3S,5S)-8-Methyl-3-p-tolyl-8-aza-bicyclo[3.2.1]octane-2-carbonyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,3S,5S)-8-Methyl-3-p-tolyl-8-aza-bicyclo[3.2.1]octane-2-carbonyl chloride

Chemical Property:

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Technology Process of (1R,2S,3S,5S)-8-Methyl-3-p-tolyl-8-aza-bicyclo[3.2.1]octane-2-carbonyl chloride

There total 4 articles about (1R,2S,3S,5S)-8-Methyl-3-p-tolyl-8-aza-bicyclo[3.2.1]octane-2-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 141807-59-2
8-methyl-3S-p-tolyl-8-azabicyclo[3.2.1]octane-2S-carboxylic acid

: 204071-17-0
(1R,2S,3S,5S)-8-Methyl-3-p-tolyl-8-aza-bicyclo[3.2.1]octane-2-carbonyl chloride

Guidance literature:: With thionyl chloride;
DOI:10.1021/jm00091a019

Reference yield:

: 130342-81-3
RTI-32

: 204071-17-0
(1R,2S,3S,5S)-8-Methyl-3-p-tolyl-8-aza-bicyclo[3.2.1]octane-2-carbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: H₂O / dioxane / Heating

2: POCl₃

With water; trichlorophosphate; In 1,4-dioxane;
DOI:10.1016/S0960-894X(01)00626-6

Reference yield:

: 4294-57-9
para-methylphenylmagnesium bromide

: 204071-17-0
(1R,2S,3S,5S)-8-Methyl-3-p-tolyl-8-aza-bicyclo[3.2.1]octane-2-carbonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether

2: H₂O / dioxane / Heating

3: POCl₃

With water; trichlorophosphate; In 1,4-dioxane; diethyl ether;
DOI:10.1016/S0960-894X(01)00626-6