(E,3R,5R)-5-(tert-butyl-diphenyl-silanyloxy)-7-methoxycarbonyl-3-methyl-6-heptenyl benzoate

Base Information

Chemical Name:(E,3R,5R)-5-(tert-butyl-diphenyl-silanyloxy)-7-methoxycarbonyl-3-methyl-6-heptenyl benzoate
CAS No.:1228447-71-9
Molecular Formula:C₃₃H₄₀O₅Si
Molecular Weight:544.763
Hs Code.:

Synonyms:(E,3R,5R)-5-(tert-butyl-diphenyl-silanyloxy)-7-methoxycarbonyl-3-methyl-6-heptenyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E,3R,5R)-5-(tert-butyl-diphenyl-silanyloxy)-7-methoxycarbonyl-3-methyl-6-heptenyl benzoate

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Technology Process of (E,3R,5R)-5-(tert-butyl-diphenyl-silanyloxy)-7-methoxycarbonyl-3-methyl-6-heptenyl benzoate

There total 1 articles about (E,3R,5R)-5-(tert-butyl-diphenyl-silanyloxy)-7-methoxycarbonyl-3-methyl-6-heptenyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1228447-69-5
(E,3R,5R)-7-(methoxycarbonyl)-5-hydroxy-3-methylhept-6-enyl benzoate

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1228447-71-9
(E,3R,5R)-5-(tert-butyl-diphenyl-silanyloxy)-7-methoxycarbonyl-3-methyl-6-heptenyl benzoate

Guidance literature:: With 1H-imidazole; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2010.02.044

Reference yield: 45.0%

: 1228447-71-9
(E,3R,5R)-5-(tert-butyl-diphenyl-silanyloxy)-7-methoxycarbonyl-3-methyl-6-heptenyl benzoate

: 1228447-73-1
(E,4R,6R)-6-methyl-4-(tert-butyl-diphenyl-silanyloxy)-2-octene-1,8-diol

Guidance literature:: (E,3R,5R)-5-(tert-butyl-diphenyl-silanyloxy)-7-methoxycarbonyl-3-methyl-6-heptenyl benzoate; With diisobutylaluminium hydride; In diethyl ether; cyclohexane; at -78 ℃; Inert atmosphere;

With water; In diethyl ether; cyclohexane;
DOI:10.1016/j.bmc.2010.02.044