Boc-Val-ΔPhe-DL-Phe(β-OH)-OH

Base Information

Chemical Name:Boc-Val-ΔPhe-DL-Phe(β-OH)-OH
CAS No.:186030-18-2
Molecular Formula:C₂₈H₃₅N₃O₇
Molecular Weight:525.602
Hs Code.:

Synonyms:Boc-Val-ΔPhe-DL-Phe(β-OH)-OH

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Chemical Property of Boc-Val-ΔPhe-DL-Phe(β-OH)-OH

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Technology Process of Boc-Val-ΔPhe-DL-Phe(β-OH)-OH

There total 4 articles about Boc-Val-ΔPhe-DL-Phe(β-OH)-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69-96-5
Phenylserin

: 124194-30-5
Boc-Val-Δ^ZPhe azlactone

: 186030-18-2
Boc-Val-ΔPhe-DL-Phe(β-OH)-OH

Guidance literature:: With sodium hydroxide; In water; acetone; at 20 ℃; for 24h;
DOI:10.1021/ja961460o

Reference yield:

: 13734-41-3
t-Boc-L-valine

: 186030-18-2
Boc-Val-ΔPhe-DL-Phe(β-OH)-OH

Guidance literature:: Multi-step reaction with 3 steps

1.1: isobutylchloroformate; N-methylmorpholine / tetrahydrofuran / 0.17 h / -10 °C

1.2: 80 percent / NaOH / tetrahydrofuran; H₂O / 0 - 20 °C

2.1: 75 percent / acetic anhydride; sodium acetate / 20 h / 20 °C

3.1: NaOH / H₂O; acetone / 24 h / 20 °C

With 4-methyl-morpholine; sodium hydroxide; sodium acetate; acetic anhydride; isobutyl chloroformate; In tetrahydrofuran; water; acetone; 1.1: Condensation / 1.2: Condensation / 2.1: azlactonization / 3.1: Condensation;
DOI:10.1021/ja961460o

Reference yield:

: 69-96-5
Phenylserin

: 186030-18-2
Boc-Val-ΔPhe-DL-Phe(β-OH)-OH

Guidance literature:: Multi-step reaction with 3 steps

1.1: isobutylchloroformate; N-methylmorpholine / tetrahydrofuran / 0.17 h / -10 °C

1.2: 80 percent / NaOH / tetrahydrofuran; H₂O / 0 - 20 °C

2.1: 75 percent / acetic anhydride; sodium acetate / 20 h / 20 °C

3.1: NaOH / H₂O; acetone / 24 h / 20 °C

With 4-methyl-morpholine; sodium hydroxide; sodium acetate; acetic anhydride; isobutyl chloroformate; In tetrahydrofuran; water; acetone; 1.1: Condensation / 1.2: Condensation / 2.1: azlactonization / 3.1: Condensation;
DOI:10.1021/ja961460o