O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranosyl)-(1-4)-O-(2-O-acetyl-3-O-benzyl-6-O-(chloroacetyl)-α-D-mannopyranosyl)-(1-4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1-6)-1-O-allyl-2,3,4,5-tetra-O-benzyl-D-myo-inosito

Base Information

• Chemical Name: O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranosyl)-(1-4)-O-(2-O-acetyl-3-O-benzyl-6-O-(chloroacetyl)-α-D-mannopyranosyl)-(1-4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1-6)-1-O-allyl-2,3,4,5-tetra-O-benzyl-D-myo-inosito
• CAS No.: 150772-59-1
• Molecular Formula: C₁₀₃H₁₁₁ClN₄O₂₂
• Molecular Weight: 1792.48

Synonyms:O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranosyl)-(1-4)-O-(2-O-acetyl-3-O-benzyl-6-O-(chloroacetyl)-α-D-mannopyranosyl)-(1-4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1-6)-1-O-allyl-2,3,4,5-tetra-O-benzyl-D-myo-inosito

Chemical Property of O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranosyl)-(1-4)-O-(2-O-acetyl-3-O-benzyl-6-O-(chloroacetyl)-α-D-mannopyranosyl)-(1-4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1-6)-1-O-allyl-2,3,4,5-tetra-O-benzyl-D-myo-inosito

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Technology Process of O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranosyl)-(1-4)-O-(2-O-acetyl-3-O-benzyl-6-O-(chloroacetyl)-α-D-mannopyranosyl)-(1-4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1-6)-1-O-allyl-2,3,4,5-tetra-O-benzyl-D-myo-inosito

There total 3 articles about O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranosyl)-(1-4)-O-(2-O-acetyl-3-O-benzyl-6-O-(chloroacetyl)-α-D-mannopyranosyl)-(1-4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1-6)-1-O-allyl-2,3,4,5-tetra-O-benzyl-D-myo-inosito which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

triethylsilyl trifluoroacetate (562-98-1) + (2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-1-O-allyl-2,3,4,5-tetra-O-benzyl-D-myo-inositol (150772-66-0) → O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranosyl)-(1-4)-O-(2-O-acetyl-3-O-benzyl-6-O-(chloroacetyl)-α-D-mannopyranosyl)-(1-4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1-6)-1-O-allyl-2,3,4,5-tetra-O-benzyl-D-myo-inosito (150772-59-1) + [(2R,3S,4R,5R,6R)-6-((1S,2R,3S,4S,5R,6S)-2-Allyloxy-3,4,5,6-tetrakis-benzyloxy-cyclohexyloxy)-5-azido-4-benzyloxy-2-benzyloxymethyl-tetrahydro-pyran-3-yloxy]-triethyl-silane

Guidance literature:

With N-iodo-succinimide; pent-4-enyl 4-O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranosyl)-2-O-acetyl-3-O-benzyl-6-O-(chloroacetyl)-α-D-mannopyranoside; In dichloromethane; for 0.25h; Ambient temperature;

DOI:10.1021/ja00110a011

Reference yield: 55.0%

pent-4-enyl 4-O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranosyl)-2-O-acetyl-3-O-benzyl-6-O-(chloroacetyl)-α-D-mannopyranoside (150772-65-9) + (2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-1-O-allyl-2,3,4,5-tetra-O-benzyl-D-myo-inositol (150772-66-0) → O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranosyl)-(1-4)-O-(2-O-acetyl-3-O-benzyl-6-O-(chloroacetyl)-α-D-mannopyranosyl)-(1-4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1-6)-1-O-allyl-2,3,4,5-tetra-O-benzyl-D-myo-inosito (150772-59-1)

Guidance literature:

With N-iodo-succinimide; triethylsilyl trifluoromethyl sulfonate; In dichloromethane; for 0.25h; Ambient temperature;

DOI:10.1021/ja00070a048

Reference yield:

pent-4-enyl 4-O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranosyl)-2-O-acetyl-3-O-benzyl-6-O-(chloroacetyl)-α-D-mannopyranoside (150772-65-9) + (2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-1-O-allyl-2,3,4,5-tetra-O-benzyl-D-myo-inositol (150772-66-0) → O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranosyl)-(1-4)-O-(2-O-acetyl-3-O-benzyl-6-O-(chloroacetyl)-α-D-mannopyranosyl)-(1-4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1-6)-1-O-allyl-2,3,4,5-tetra-O-benzyl-D-myo-inosito (150772-59-1) + [(2R,3S,4R,5R,6R)-6-((1S,2R,3S,4S,5R,6S)-2-Allyloxy-3,4,5,6-tetrakis-benzyloxy-cyclohexyloxy)-5-azido-4-benzyloxy-2-benzyloxymethyl-tetrahydro-pyran-3-yloxy]-triethyl-silane

Guidance literature:

With N-iodo-succinimide; triethylsilyl trifluoromethyl sulfonate; In dichloromethane; for 0.25h; Ambient temperature;

DOI:10.1021/ja00110a011

upstream raw materials:

pent-4-enyl 4-O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranosyl)-2-O-acetyl-3-O-benzyl-6-O-(chloroacetyl)-α-D-mannopyranoside

(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-1-O-allyl-2,3,4,5-tetra-O-benzyl-D-myo-inositol

triethylsilyl trifluoroacetate

Downstream raw materials:

O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranosyl)-(1-4)-O-(2-O-acetyl-3-O-benzyl-α-D-mannopyranosyl)-(1-4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1-6)-1-O-allyl-2,3,4,5-tetra-O-benzyl-D-myo-inositol

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