benzyl (S)-3-amino>-3-(4-biphenylyl)propionyl>amino>propionate

Base Information

Chemical Name:benzyl (S)-3-amino>-3-(4-biphenylyl)propionyl>amino>propionate
CAS No.:155873-49-7
Molecular Formula:C₂₈H₃₃N₂O₆P
Molecular Weight:524.554
Hs Code.:

benzyl (S)-3-<N-<2-<<(dimethylphosphono)methyl>amino>-3-(4-biphenylyl)propionyl>amino>propionate

Synonyms:benzyl (S)-3-amino>-3-(4-biphenylyl)propionyl>amino>propionate

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Chemical Property of benzyl (S)-3-amino>-3-(4-biphenylyl)propionyl>amino>propionate

Chemical Property:

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Technology Process of benzyl (S)-3-amino>-3-(4-biphenylyl)propionyl>amino>propionate

There total 3 articles about benzyl (S)-3-amino>-3-(4-biphenylyl)propionyl>amino>propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.7%

: 27019-47-2
β-alanine benzyl ester p-toluenesulfonate

: 147862-23-5
(S)-2-amino>-3-(4-biphenylyl)propionic acid

: 155873-49-7
benzyl (S)-3-amino>-3-(4-biphenylyl)propionyl>amino>propionate

Guidance literature:: With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; for 10h; Ambient temperature;

Reference yield:

: (S)-4-phenylphenylalanine benzyl ester

: 155873-49-7
benzyl (S)-3-amino>-3-(4-biphenylyl)propionyl>amino>propionate

Guidance literature:: Multi-step reaction with 3 steps

1: 92.5 percent / diisopropylethylamine / CH₂Cl₂ / 18 h / Ambient temperature

2: 88 percent / H₂ / 10percent Pd/C / ethyl acetate / 2 h / 2585.7 Torr

3: 99.7 percent / Et₃N, 1-hydroxybenzotriazole (HOBt), 4-(dimethylamino)pyridine (DMAP), N-<3-(dimethylamino)propyl>-N'-ethylcarbodiimide hydrochloride (EDC) / dimethylformamide / 10 h / Ambient temperature

With dmap; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 155873-61-3
benzyl (S)-2-amino>-3-(4-biphenylyl)propionate

: 155873-49-7
benzyl (S)-3-amino>-3-(4-biphenylyl)propionyl>amino>propionate

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / H₂ / 10percent Pd/C / ethyl acetate / 2 h / 2585.7 Torr

2: 99.7 percent / Et₃N, 1-hydroxybenzotriazole (HOBt), 4-(dimethylamino)pyridine (DMAP), N-<3-(dimethylamino)propyl>-N'-ethylcarbodiimide hydrochloride (EDC) / dimethylformamide / 10 h / Ambient temperature

With dmap; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide;