2-[2-(3-{[2-(benzyloxy)acetamido]methyl}benzylamino)-2-oxoethoxy]N,N-dioctylacetamide

Base Information

Chemical Name:2-[2-(3-{[2-(benzyloxy)acetamido]methyl}benzylamino)-2-oxoethoxy]N,N-dioctylacetamide
CAS No.:1355069-43-0
Molecular Formula:C₃₇H₅₇N₃O₅
Molecular Weight:623.877
Hs Code.:

Synonyms:2-[2-(3-{[2-(benzyloxy)acetamido]methyl}benzylamino)-2-oxoethoxy]N,N-dioctylacetamide

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Chemical Property of 2-[2-(3-{[2-(benzyloxy)acetamido]methyl}benzylamino)-2-oxoethoxy]N,N-dioctylacetamide

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Technology Process of 2-[2-(3-{[2-(benzyloxy)acetamido]methyl}benzylamino)-2-oxoethoxy]N,N-dioctylacetamide

There total 4 articles about 2-[2-(3-{[2-(benzyloxy)acetamido]methyl}benzylamino)-2-oxoethoxy]N,N-dioctylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1355069-37-2
C₁₇H₂₀N₂O₂

: 135447-09-5
2-(2-(di-octylamino)-2-oxoethoxy)acetic acid

: 1355069-43-0
2-[2-(3-{[2-(benzyloxy)acetamido]methyl}benzylamino)-2-oxoethoxy]N,N-dioctylacetamide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1002/ejoc.201100443

Reference yield:

: 1027755-54-9
2-dioctylcarbamoylmethoxy-N-[3-[(2-dioctyl-carbamoylmethoxy-acetylamino)methyl]benzyl]acetamide

: 1355069-43-0
2-[2-(3-{[2-(benzyloxy)acetamido]methyl}benzylamino)-2-oxoethoxy]N,N-dioctylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: dodecane; octanol / Irradiation

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 48 h / 20 °C / Inert atmosphere

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dodecane; octanol; dichloromethane;
DOI:10.1002/ejoc.201100443

Reference yield:

: 30379-55-6
benzyloxyacetic acid

: 1355069-43-0
2-[2-(3-{[2-(benzyloxy)acetamido]methyl}benzylamino)-2-oxoethoxy]N,N-dioctylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere

2: trifluoroacetic acid

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 48 h / 20 °C / Inert atmosphere

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1002/ejoc.201100443