allyl 2-amino-4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-α-D-allopyranoside

Base Information

Chemical Name:allyl 2-amino-4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-α-D-allopyranoside
CAS No.:1418181-38-0
Molecular Formula:C₁₇H₁₉NO₆
Molecular Weight:333.341
Hs Code.:

Synonyms:allyl 2-amino-4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-α-D-allopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl 2-amino-4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-α-D-allopyranoside

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Technology Process of allyl 2-amino-4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-α-D-allopyranoside

There total 2 articles about allyl 2-amino-4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-α-D-allopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₄N₂O₉

: 1418181-38-0
allyl 2-amino-4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-α-D-allopyranoside

Guidance literature:: With sodium hydride; 4-Nitrophenyl chloroformate; In N,N-dimethyl-formamide; mineral oil; at 30 ℃; for 0.75h;
DOI:10.1016/j.tet.2012.12.005

Reference yield:

: 136773-79-0
Allyl 2-Amino-4,6-O-benzylidene-2-deoxy-α-D-allopyranoside

: 1418181-38-0
allyl 2-amino-4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-α-D-allopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / acetonitrile; water / 0.5 h / 0 °C

2: 4-Nitrophenyl chloroformate; sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 30 °C

With sodium hydride; sodium hydrogencarbonate; 4-Nitrophenyl chloroformate; In water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1016/j.tet.2012.12.005