6,8-Di-O-Benzyl-3-C-(benzyloxymethyl)-3,5,7,9-tetradeoxy-1,2-O-isopropylidene-5,7,9-tri-C-methyl-α-D-altro-L-talo-decodialdofuranose-(1,4)

Base Information

• Chemical Name: 6,8-Di-O-Benzyl-3-C-(benzyloxymethyl)-3,5,7,9-tetradeoxy-1,2-O-isopropylidene-5,7,9-tri-C-methyl-α-D-altro-L-talo-decodialdofuranose-(1,4)
• CAS No.: 104107-53-1
• Molecular Formula: C₃₈H₄₈O₇
• Molecular Weight: 616.795

Synonyms:6,8-Di-O-Benzyl-3-C-(benzyloxymethyl)-3,5,7,9-tetradeoxy-1,2-O-isopropylidene-5,7,9-tri-C-methyl-α-D-altro-L-talo-decodialdofuranose-(1,4)

Chemical Property of 6,8-Di-O-Benzyl-3-C-(benzyloxymethyl)-3,5,7,9-tetradeoxy-1,2-O-isopropylidene-5,7,9-tri-C-methyl-α-D-altro-L-talo-decodialdofuranose-(1,4)

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Technology Process of 6,8-Di-O-Benzyl-3-C-(benzyloxymethyl)-3,5,7,9-tetradeoxy-1,2-O-isopropylidene-5,7,9-tri-C-methyl-α-D-altro-L-talo-decodialdofuranose-(1,4)

There total 3 articles about 6,8-Di-O-Benzyl-3-C-(benzyloxymethyl)-3,5,7,9-tetradeoxy-1,2-O-isopropylidene-5,7,9-tri-C-methyl-α-D-altro-L-talo-decodialdofuranose-(1,4) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

6,8-Di-O-Benzyl-3-C-(benzyloxymethyl)-3,5,7,9-tetradeoxy-1,2-O-isopropylidene-5,7,9-tri-C-methyl-α-D-glycero-D-altro-L-talo-undecofuranose-(1,4) (131755-70-9) → 6,8-Di-O-Benzyl-3-C-(benzyloxymethyl)-3,5,7,9-tetradeoxy-1,2-O-isopropylidene-5,7,9-tri-C-methyl-α-D-altro-L-talo-decodialdofuranose-(1,4) (104107-53-1)

Guidance literature:

With lead(IV) acetate; potassium acetate; In acetonitrile; at 0 ℃; for 0.5h;

DOI:10.1016/S0040-4020(01)85586-1

Reference yield: 97.0%

6,8-di-O-benzyl-3-C-(benzyloxymethyl)-3,5,7,9,12-pentadeoxy-1,2-O-isopropylidene-5,7,9-tri-C-methyl-D-erythro-D-altro-L-talo-dodecofuranose-(1,4) → 6,8-Di-O-Benzyl-3-C-(benzyloxymethyl)-3,5,7,9-tetradeoxy-1,2-O-isopropylidene-5,7,9-tri-C-methyl-α-D-altro-L-talo-decodialdofuranose-(1,4) (104107-53-1)

Guidance literature:

With sodium periodate; In water; acetone; for 5h; Ambient temperature;

DOI:10.1246/bcsj.58.3457

Reference yield:

6,8-di-O-benzyl-3-C-(benzyloxymethyl)-3,5,7,9,12-pentadeoxy-1,2-O-isopropylidene-5,7,9-tri-C-methyl-11-methylene-D-glycero-D-altro-β-L-talo-dodecodialdofuranose-(1,4) 12-(diethyl acetal) (104107-55-3) → 6,8-Di-O-Benzyl-3-C-(benzyloxymethyl)-3,5,7,9-tetradeoxy-1,2-O-isopropylidene-5,7,9-tri-C-methyl-α-D-altro-L-talo-decodialdofuranose-(1,4) (104107-53-1)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1016/S0040-4020(01)85586-1

upstream raw materials:

6,8-Di-O-Benzyl-3-C-(benzyloxymethyl)-3,5,7,9-tetradeoxy-1,2-O-isopropylidene-5,7,9-tri-C-methyl-α-D-glycero-D-altro-L-talo-undecofuranose-(1,4)

6,8-di-O-benzyl-3-C-(benzyloxymethyl)-3,5,7,9,12-pentadeoxy-1,2-O-isopropylidene-5,7,9-tri-C-methyl-11-methylene-D-glycero-D-altro-β-L-talo-dodecodialdofuranose-(1,4) 12-(diethyl acetal)

Downstream raw materials:

6,8-di-O-benzyl-3-C-(benzyloxymethyl)-3,5,7,9,12-pentadeoxy-1,2-O-isopropylidene-5,7,9-tri-C-methyl-11-methylene-D-glycero-D-altro-β-L-talo-dodecodialdofuranose-(1,4) 12-(diethyl acetal)

6,8-di-O-benzyl-3-C-(benzyloxymethyl)-3,5,7,9,12-pentadeoxy-1,2-O-isopropylidene-5,7,9-tri-C-methyl-11-methylene-L-glycero-D-altro-β-L-talo-dodecodialdofuranose-(1,4) 12-(diethyl acetal)

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