benzyl (S)-2-(bis(tert-butoxycarbonyl)amino)-5-oxo-6-(phenylsulfonyl)hexylcarbamate

Base Information

Chemical Name:benzyl (S)-2-(bis(tert-butoxycarbonyl)amino)-5-oxo-6-(phenylsulfonyl)hexylcarbamate
CAS No.:1133960-16-3
Molecular Formula:C₃₀H₄₀N₂O₉S
Molecular Weight:604.722
Hs Code.:

Synonyms:benzyl (S)-2-(bis(tert-butoxycarbonyl)amino)-5-oxo-6-(phenylsulfonyl)hexylcarbamate

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Chemical Property of benzyl (S)-2-(bis(tert-butoxycarbonyl)amino)-5-oxo-6-(phenylsulfonyl)hexylcarbamate

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Technology Process of benzyl (S)-2-(bis(tert-butoxycarbonyl)amino)-5-oxo-6-(phenylsulfonyl)hexylcarbamate

There total 1 articles about benzyl (S)-2-(bis(tert-butoxycarbonyl)amino)-5-oxo-6-(phenylsulfonyl)hexylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 3112-85-4
methylphenylsulfonate

: 1133960-13-0
(S)-benzyl 5-(bis(tert-butoxycarbonyl)amino)-2-oxopiperidine-1-carboxylate

: 1133960-16-3
benzyl (S)-2-(bis(tert-butoxycarbonyl)amino)-5-oxo-6-(phenylsulfonyl)hexylcarbamate

Guidance literature:: methylphenylsulfonate; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.833333h; Inert atmosphere;

(S)-benzyl 5-(bis(tert-butoxycarbonyl)amino)-2-oxopiperidine-1-carboxylate; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.3987/COM-08-S(F)37

Reference yield: 23.0%

: 1133960-16-3
benzyl (S)-2-(bis(tert-butoxycarbonyl)amino)-5-oxo-6-(phenylsulfonyl)hexylcarbamate

: 1133960-20-9
(2S,5S)-5-(bis(tert-butoxycarbonyl)amino)-2-(phenylsulfonylmethyl)piperidine

: 1133960-19-6
(2R,5S)-5-(bis(tert-butoxycarbonyl)amino)-2-(phenylsulfonylmethyl)piperidine

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 56h; under 760.051 Torr; optical yield given as %de;
DOI:10.3987/COM-08-S(F)37