allyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:allyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:85386-54-5
Molecular Formula:C₅₂H₅₇NO₁₂
Molecular Weight:888.024
Hs Code.:

Synonyms:allyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of allyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

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Technology Process of allyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 2 articles about allyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 85386-52-3
allyl O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->2)-O-(3,6-di-O-benzyl-4-O-(tetrahydropyran-2-yl)-β-D-galactopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 85386-54-5
allyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With acetic acid; In methanol; water; for 1h; Heating;
DOI:10.1016/0008-6215(83)88171-3

Reference yield:

: 85386-51-2
allyl O-(3,6-di-O-benzyl-4-O-(tetrahydropyran-2-yl)-β-D-galactopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 85386-54-5
allyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: tetraethylammonium bromide / CH₂Cl₂; dimethylformamide / 96 h / Ambient temperature

2: 88 percent / 80percent aqueous acetic acid / methanol; H₂O / 1 h / Heating

With tetraethylammonium bromide; acetic acid; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(83)88171-3

Reference yield: 64.0%

: 53081-30-4
tetra-O-benzyl-α-D-galactosyl bromide

: 85386-54-5
allyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 85395-69-3
allyl O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->4)-O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; silver carbonate; In dichloromethane; 1.) -25 deg C, 3 h; 2.) 5 deg C, overnight;
DOI:10.1016/0008-6215(83)88171-3