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Technology Process of ZnCl2CH(COOH)(C(C6H5)(CH2COOH)NHCC(CH3)N(CH3)N(C6H5)CN)(CH2)3(NCN(C6H5)N(CH3)C(CH3)CN)CC6H5

ZnCl2CH(COOH)(C(C6H5)(CH2COOH)NHCC(CH3)N(CH3)N(C6H5)CN)(CH2)3(NCN(C6H5)N(CH3)C(CH3)CN)CC6H5

Base Information
  • Chemical Name:ZnCl2CH(COOH)(C(C6H5)(CH2COOH)NHCC(CH3)N(CH3)N(C6H5)CN)(CH2)3(NCN(C6H5)N(CH3)C(CH3)CN)CC6H5
  • CAS No.:688739-24-4
  • Molecular Formula:C43H44Cl2N8O4Zn
  • Molecular Weight:873.17
  • Hs Code.:
ZnCl<sub>2</sub>CH(COOH)(C(C<sub>6</sub>H<sub>5</sub>)(CH<sub>2</sub>COOH)NHCC(CH<sub>3</sub>)N(CH<sub>3</sub>)N(C<sub>6</sub>H<sub>5</sub>)CN)(CH<sub>2</sub>)3(NCN(C<sub>6</sub>H<sub>5</sub>)N(CH<sub>3</sub>)C(CH<sub>3</sub>)CN)CC<sub>6</sub>H<sub>5</sub>

Synonyms:ZnCl2CH(COOH)(C(C6H5)(CH2COOH)NHCC(CH3)N(CH3)N(C6H5)CN)(CH2)3(NCN(C6H5)N(CH3)C(CH3)CN)CC6H5

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Chemical Property of ZnCl2CH(COOH)(C(C6H5)(CH2COOH)NHCC(CH3)N(CH3)N(C6H5)CN)(CH2)3(NCN(C6H5)N(CH3)C(CH3)CN)CC6H5
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Technology Process of ZnCl2CH(COOH)(C(C6H5)(CH2COOH)NHCC(CH3)N(CH3)N(C6H5)CN)(CH2)3(NCN(C6H5)N(CH3)C(CH3)CN)CC6H5

There total 1 articles about ZnCl2CH(COOH)(C(C6H5)(CH2COOH)NHCC(CH3)N(CH3)N(C6H5)CN)(CH2)3(NCN(C6H5)N(CH3)C(CH3)CN)CC6H5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

zinc(II) chloride hydrate

zinc(II) chloride hydrate

4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one
83-07-8

4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one

3-oxo-3-phenylpropionic acid
614-20-0

3-oxo-3-phenylpropionic acid

Trimethylenediamine
109-76-2,54018-94-9

Trimethylenediamine

ZnCl<sub>2</sub>CH(COOH)(C(C<sub>6</sub>H<sub>5</sub>)(CH<sub>2</sub>COOH)NHCC(CH<sub>3</sub>)N(CH<sub>3</sub>)N(C<sub>6</sub>H<sub>5</sub>)CN)(CH<sub>2</sub>)3(NCN(C<sub>6</sub>H<sub>5</sub>)N(CH<sub>3</sub>)C(CH<sub>3</sub>)CN)CC<sub>6</sub>H<sub>5</sub>
688739-24-4

ZnCl2CH(COOH)(C(C6H5)(CH2COOH)NHCC(CH3)N(CH3)N(C6H5)CN)(CH2)3(NCN(C6H5)N(CH3)C(CH3)CN)CC6H5

Guidance literature:
With HCl; In ethanol; mixt. of 4-aminoantipyrine and diamine refluxed for 20 h, cooled to 0 °C, HCl added, ppt. redissolved in hot ethanol, benzoylacetic acid added, refluxed for 30 min, cooled to 0 °C, metal salt added; ppt. filtered, washed (cold ethanol), dried (vac.); elem. anal.;
DOI:10.1081/SIM-120026552
upstream raw materials:

4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one

3-oxo-3-phenylpropionic acid

Trimethylenediamine

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