2-(((2S,3aS,4R,6S,6aR)-6-(6-(3-ethylureido)-9H-purin-9-yl)-2-styryltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)acetic acid

Base Information

• Chemical Name: 2-(((2S,3aS,4R,6S,6aR)-6-(6-(3-ethylureido)-9H-purin-9-yl)-2-styryltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)acetic acid
• CAS No.: 1024677-54-0
• Molecular Formula: C₂₄H₂₆N₆O₆S
• Molecular Weight: 526.573

Synonyms:2-(((2S,3aS,4R,6S,6aR)-6-(6-(3-ethylureido)-9H-purin-9-yl)-2-styryltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)acetic acid

Chemical Property of 2-(((2S,3aS,4R,6S,6aR)-6-(6-(3-ethylureido)-9H-purin-9-yl)-2-styryltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)acetic acid

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Technology Process of 2-(((2S,3aS,4R,6S,6aR)-6-(6-(3-ethylureido)-9H-purin-9-yl)-2-styryltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)acetic acid

There total 1 articles about 2-(((2S,3aS,4R,6S,6aR)-6-(6-(3-ethylureido)-9H-purin-9-yl)-2-styryltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

((2S,3aS,4R,6R,6aS)-6-(6-(3-etylureido)-9H-purin-9-yl)-2-styryl-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methyl 4-methylbenzenesulfonate (1024676-67-2) + mercaptoacetic acid (68-11-1) → 2-(((2S,3aS,4R,6S,6aR)-6-(6-(3-ethylureido)-9H-purin-9-yl)-2-styryltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)acetic acid (1024677-54-0)

Guidance literature:

With potassium tert-butylate; In dimethyl sulfoxide; at 25 - 30 ℃; for 24h;

DOI:10.1016/j.bmcl.2008.01.038

Reference yield: 20.0%

2-(((2S,3aS,4R,6S,6aR)-6-(6-(3-ethylureido)-9H-purin-9-yl)-2-styryltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)acetic acid (1024677-54-0) → 2-(((2S,3aS,4R,6S,6aR)-6-(6-(3-ethylureido)-9H-purin-9-yl)-2-styryltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylsulfonyl)acetic acid (1024677-57-3)

Guidance literature:

With oxone; potassium carbonate; In methanol; at 20 ℃; pH=5;

DOI:10.1016/j.bmcl.2008.01.038

upstream raw materials:

((2S,3aS,4R,6R,6aS)-6-(6-(3-etylureido)-9H-purin-9-yl)-2-styryl-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methyl 4-methylbenzenesulfonate

mercaptoacetic acid

Downstream raw materials:

2-(((2S,3aS,4R,6S,6aR)-6-(6-(3-ethylureido)-9H-purin-9-yl)-2-styryltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylsulfonyl)acetic acid

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