4-(4,5-dibromo-1H-pyrrole-2-carbonyl)-2-phenylsulfanyl-4,5,6,7-tetrahydro-imidazo[4,5-b]pyridine-1-sulfonic acid dimethylamide

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Chemical Name:4-(4,5-dibromo-1H-pyrrole-2-carbonyl)-2-phenylsulfanyl-4,5,6,7-tetrahydro-imidazo[4,5-b]pyridine-1-sulfonic acid dimethylamide
CAS No.:1146689-51-1
Molecular Formula:C₁₉H₁₉Br₂N₅O₃S₂
Molecular Weight:589.332
Hs Code.:

Synonyms:4-(4,5-dibromo-1H-pyrrole-2-carbonyl)-2-phenylsulfanyl-4,5,6,7-tetrahydro-imidazo[4,5-b]pyridine-1-sulfonic acid dimethylamide

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Chemical Property of 4-(4,5-dibromo-1H-pyrrole-2-carbonyl)-2-phenylsulfanyl-4,5,6,7-tetrahydro-imidazo[4,5-b]pyridine-1-sulfonic acid dimethylamide

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Technology Process of 4-(4,5-dibromo-1H-pyrrole-2-carbonyl)-2-phenylsulfanyl-4,5,6,7-tetrahydro-imidazo[4,5-b]pyridine-1-sulfonic acid dimethylamide

There total 1 articles about 4-(4,5-dibromo-1H-pyrrole-2-carbonyl)-2-phenylsulfanyl-4,5,6,7-tetrahydro-imidazo[4,5-b]pyridine-1-sulfonic acid dimethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1146689-69-1
4-[4,5-dibromo-1-(2-trimethylsilanyl-ethoxymethyl)-1H-pyrrole-2-carbonyl]-2-phenylsulfanyl-4,5,6,7-tetrahydro-imidazo[4,5-b]pyridine-1-sulfonic acid dimethylamide

: 1146689-51-1
4-(4,5-dibromo-1H-pyrrole-2-carbonyl)-2-phenylsulfanyl-4,5,6,7-tetrahydro-imidazo[4,5-b]pyridine-1-sulfonic acid dimethylamide

Guidance literature:: 4-[4,5-dibromo-1-(2-trimethylsilanyl-ethoxymethyl)-1H-pyrrole-2-carbonyl]-2-phenylsulfanyl-4,5,6,7-tetrahydro-imidazo[4,5-b]pyridine-1-sulfonic acid dimethylamide; With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

With water; Further stages; Cooling with ice;
DOI:10.1021/jo900283g

Reference yield: 66.0%

: 1146689-51-1
4-(4,5-dibromo-1H-pyrrole-2-carbonyl)-2-phenylsulfanyl-4,5,6,7-tetrahydro-imidazo[4,5-b]pyridine-1-sulfonic acid dimethylamide

: 3a,10,11,12-tetrabromo-3a,4,5,6-tetrahydro-N,N-dimethyl-2-(phenylthio)-8-oxo-3H,8H-imidazo[4,5-b]pyrrolo[1',2':3,4]imidazo[1,2-a]pyridine-3-sulfonamide

Guidance literature:: With N-chloro-succinimide; lithium bromide; In tetrahydrofuran; dichloromethane; for 0.0833333h; Inert atmosphere;
DOI:10.1021/jo900283g