Technology Process of C19H15N3
There total 3 articles about C19H15N3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanol; ammonium chloride; zinc;
In
dichloromethane;
at 50 ℃;
for 6h;
Solvent;
Temperature;
Time;
DOI:10.1021/ol303434n
- Guidance literature:
-
Multi-step reaction with 3 steps
1: copper(I) bromide
2: palladium diacetate; tert.-butylhydroperoxide / 1,2-dichloro-ethane / 12 h / 80 °C / Inert atmosphere; Sealed tube
3: zinc; ammonium chloride; methanol / dichloromethane / 6 h / 50 °C
With
methanol; tert.-butylhydroperoxide; palladium diacetate; ammonium chloride; copper(I) bromide; zinc;
In
dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ol303434n
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium diacetate; tert.-butylhydroperoxide / 1,2-dichloro-ethane / 12 h / 80 °C / Inert atmosphere; Sealed tube
2: zinc; ammonium chloride; methanol / dichloromethane / 6 h / 50 °C
With
methanol; tert.-butylhydroperoxide; palladium diacetate; ammonium chloride; zinc;
In
dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ol303434n