Fe₂{P(C₆H₅)2}2(CO)5(COCH₃)^(1-)*Na⁽¹⁺⁾*2C₄H₈O=NaFe₂{P(C₆H₅)2}2(CO)5(COCH₃)*2C₄H₈O

Base Information

• Chemical Name: Fe₂{P(C₆H₅)2}2(CO)5(COCH₃)^(1-)*Na⁽¹⁺⁾*2C₄H₈O=NaFe₂{P(C₆H₅)2}2(CO)5(COCH₃)*2C₄H₈O
• CAS No.: 72275-07-1
• Molecular Formula: 2C₄H₈O*C₃₁H₂₃Fe₂O₆P₂*Na
• Molecular Weight: 832.365

Synonyms:Fe₂{P(C₆H₅)2}2(CO)5(COCH₃)^(1-)*Na⁽¹⁺⁾*2C₄H₈O=NaFe₂{P(C₆H₅)2}2(CO)5(COCH₃)*2C₄H₈O

Chemical Property of Fe₂{P(C₆H₅)2}2(CO)5(COCH₃)^(1-)*Na⁽¹⁺⁾*2C₄H₈O=NaFe₂{P(C₆H₅)2}2(CO)5(COCH₃)*2C₄H₈O

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Technology Process of Fe₂{P(C₆H₅)2}2(CO)5(COCH₃)^(1-)*Na⁽¹⁺⁾*2C₄H₈O=NaFe₂{P(C₆H₅)2}2(CO)5(COCH₃)*2C₄H₈O

There total 1 articles about Fe₂{P(C₆H₅)2}2(CO)5(COCH₃)^(1-)*Na⁽¹⁺⁾*2C₄H₈O=NaFe₂{P(C₆H₅)2}2(CO)5(COCH₃)*2C₄H₈O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Fe2{P(C6H5)2}2(CO)6(2-)*2Na(1+)*5C4H8O=Na2Fe2{P(C6H5)2}2(CO)6*5C4H8O (79172-61-5) + methyl p-toluene sulfonate (80-48-8) → Fe2{P(C6H5)2}2(CO)5(COCH3)(1-)*Na(1+)*2C4H8O=NaFe2{P(C6H5)2}2(CO)5(COCH3)*2C4H8O (72275-07-1)

Guidance literature:

In tetrahydrofuran; under N2, stirring about 1 week; react. mixt. filtered, slow addn. of hexane afforded red crystals, washing with hexane, elem. anal.;

DOI:10.1021/ic00131a029

Reference yield: 65.0%

Fe2{P(C6H5)2}2(CO)5(COCH3)(1-)*Na(1+)*2C4H8O=NaFe2{P(C6H5)2}2(CO)5(COCH3)*2C4H8O (72275-07-1) → Fe2{P(C6H5)2}2(CO)6(2-)*2Na(1+)*5C4H8O=Na2Fe2{P(C6H5)2}2(CO)6*5C4H8O (79172-61-5)

Guidance literature:

With sodium; In tetrahydrofuran; 50% sodium dispersion, 2 h stirring; mixture was filtered, diffusion of hexane vapor into filtrate resulted in crystals of product, washed with hexane, dried in vac.;

DOI:10.1021/ic00131a029

Reference yield: 8.0%

Fe2{P(C6H5)2}2(CO)5(COCH3)(1-)*Na(1+)*2C4H8O=NaFe2{P(C6H5)2}2(CO)5(COCH3)*2C4H8O (72275-07-1) + Dimethyl(phenyl)phosphine (672-66-2) → Fe2{P(C6H5)2}2(CO)4{P(CH3)2(C6H5)}2 (79172-60-4) + Fe2{P(C6H5)2}2(CO)5{P(CH3)2(C6H5)} (79172-57-9)

Guidance literature:

In dimethylsulfoxide-d6; under N2 sealed in NMR tube, 1h at 100°; addn. of THF, pptn. of Fe2(PPh2)(CO)42, elem. anal., chromy. in air of filtrate from crystn., major band sraped from the plate, washed with benzene, filtered, solvent removed under reduced pressure affording Fe2(PPh2)2(CO)5;

DOI:10.1021/ic00131a029

upstream raw materials:

Fe₂{P(C₆H₅)2}2(CO)6^(2-)*2Na⁽¹⁺⁾*5C₄H₈O=Na₂Fe₂{P(C₆H₅)2}2(CO)6*5C₄H₈O

methyl p-toluene sulfonate

Downstream raw materials:

Fe₂{P(C₆H₅)2}2(CO)4{P(CH₃)2(C₆H₅)}2

Fe₂{P(C₆H₅)2}2(CO)5{P(CH₃)2(C₆H₅)}

Fe₂{P(C₆H₅)2}2(CO)6^(2-)*2Na⁽¹⁺⁾*5C₄H₈O=Na₂Fe₂{P(C₆H₅)2}2(CO)6*5C₄H₈O

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