N⁶,N⁶,O^2',O^3'-tetrabenzoyl-5'-deoxy-5'-(N¹,N³-diphenylethylenediamino)adenosine

Base Information

• Chemical Name: N⁶,N⁶,O^2',O^3'-tetrabenzoyl-5'-deoxy-5'-(N¹,N³-diphenylethylenediamino)adenosine
• CAS No.: 100899-70-5
• Molecular Formula: C₅₂H₄₁N₇O₇
• Molecular Weight: 875.94

Synonyms:N⁶,N⁶,O^2',O^3'-tetrabenzoyl-5'-deoxy-5'-(N¹,N³-diphenylethylenediamino)adenosine

Chemical Property of N⁶,N⁶,O^2',O^3'-tetrabenzoyl-5'-deoxy-5'-(N¹,N³-diphenylethylenediamino)adenosine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N⁶,N⁶,O^2',O^3'-tetrabenzoyl-5'-deoxy-5'-(N¹,N³-diphenylethylenediamino)adenosine

There total 1 articles about N⁶,N⁶,O^2',O^3'-tetrabenzoyl-5'-deoxy-5'-(N¹,N³-diphenylethylenediamino)adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N6,N6,O2',O3'-tetrabenzoyladenosine 5'-aldehyde (100899-71-6) + N,N'-diphenylethylenediamine (150-61-8) → N6,N6,O2',O3'-tetrabenzoyl-5'-deoxy-5'-(N1,N3-diphenylethylenediamino)adenosine (100899-70-5)

Guidance literature:

With acetic acid; In methanol; Yield given;

DOI:10.1021/jo00358a017

Reference yield: 100.0%

N6,N6,O2',O3'-tetrabenzoyl-5'-deoxy-5'-(N1,N3-diphenylethylenediamino)adenosine (100899-70-5) → N6,N6,O2',O3'-tetrabenzoyladenosine 5'-aldehyde (100899-71-6)

Guidance literature:

With toluene-4-sulfonic acid; In dichloromethane; acetone; at 0 ℃; for 0.5h;

DOI:10.1021/jo00358a017

Reference yield:

N6,N6,O2',O3'-tetrabenzoyl-5'-deoxy-5'-(N1,N3-diphenylethylenediamino)adenosine (100899-70-5) → N6,N6,O2,O3-tetrabenzoyl-9-<5-deoxy-5-(methylthio)-β-D-erythro-(Z)-pent-4-enofuranosyl>adenine (100899-76-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 100 percent / p-toluenesulfonic acid monohydrate / acetone; CH₂Cl₂ / 0.5 h / 0 °C

2: trimethylsilyl triflate, zinc iodide / tetrahydrofuran / 2 h / Ambient temperature

3: 1.) Br₂, 2.) 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU) / 1.) CH₂Cl₂, -78 deg C, 35 min

With trimethylsilyl trifluoromethanesulfonate; bromine; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; zinc(II) iodide; In tetrahydrofuran; dichloromethane; acetone;

DOI:10.1021/jo00358a017

upstream raw materials:

N⁶,N⁶,O^2',O^3'-tetrabenzoyladenosine 5'-aldehyde

N,N'-diphenylethylenediamine

Downstream raw materials:

N⁶,N⁶,O^2',O^3'-tetrabenzoyladenosine 5'-aldehyde

N⁶,N⁶,O^2',O^3'-tetrabenzoyl-5'-deoxy-5',5'-bis(methylthio)adenosine

N⁶,N⁶,O²,O³-tetrabenzoyl-9-<5-deoxy-5-(isobutylthio)-β-D-erythro-(Z)-pent-4-enofuranosyl>adenine

N⁶,N⁶,O^2',O^3'-tetrabenzoyl-5'-deoxy-5',5'-bis(isobutylthio)adenosine

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 100899-70-5 N⁶,N⁶,O^2',O^3'-tetrabenzoyl-5'-deoxy-5'-(N¹,N³-diphenylethylenediamino)adenosine

Send

Send

Metric Ton KG G Pound L ML

Send

Send