(1R,2S,6R,7S)-4-(2-Methoxy-phenyl)-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

Base Information

• Chemical Name: (1R,2S,6R,7S)-4-(2-Methoxy-phenyl)-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione
• CAS No.: 93465-44-2
• Molecular Formula: C₁₆H₁₅NO₃
• Molecular Weight: 269.3

Synonyms:(1R,2S,6R,7S)-4-(2-Methoxy-phenyl)-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

Chemical Property of (1R,2S,6R,7S)-4-(2-Methoxy-phenyl)-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

Chemical Property:

Purity/Quality:

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Technology Process of (1R,2S,6R,7S)-4-(2-Methoxy-phenyl)-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

There total 2 articles about (1R,2S,6R,7S)-4-(2-Methoxy-phenyl)-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methoxy-phenylamine (90-04-0) + 3,6-endomethylene-1,2,3,6-tetrahydrophthalic anhydride (129-64-6) → (1R,2S,6R,7S)-4-(2-Methoxy-phenyl)-4-aza-tricyclo[5.2.1.02,6]dec-8-ene-3,5-dione (93465-44-2)

Guidance literature:

Reference yield:

C16H17NO4 (61894-11-9) → (1R,2S,6R,7S)-4-(2-Methoxy-phenyl)-4-aza-tricyclo[5.2.1.02,6]dec-8-ene-3,5-dione (93465-44-2)

Guidance literature:

at 130 ℃; for 16h; Neat (no solvent);

DOI:10.1021/ol201657p

Reference yield: 90.0%

(1R,2S,6R,7S)-4-(2-Methoxy-phenyl)-4-aza-tricyclo[5.2.1.02,6]dec-8-ene-3,5-dione (93465-44-2) → C16H15NO4 (477248-68-3)

Guidance literature:

With peracetic acid; In 1,4-dioxane; at 10 ℃;

DOI:10.1023/A:1015573902465

upstream raw materials:

2-methoxy-phenylamine

3,6-endomethylene-1,2,3,6-tetrahydrophthalic anhydride

C₁₆H₁₇NO₄

Downstream raw materials:

C₁₆H₁₅NO₄

2-exo-hydroxy-5-oxo-4-oxatricyclo[4.2.1.0^3,7]nonane-9-carboxylic acid

C₁₆H₁₇NO₅

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