1-p-chlorophenyl-6-tosyl-1,3-diazadihydroazulanone

Base Information

• Chemical Name: 1-p-chlorophenyl-6-tosyl-1,3-diazadihydroazulanone
• CAS No.: 262296-54-8
• Molecular Formula: C₂₁H₁₇ClN₂O₃S
• Molecular Weight: 412.897

Synonyms:1-p-chlorophenyl-6-tosyl-1,3-diazadihydroazulanone

Chemical Property of 1-p-chlorophenyl-6-tosyl-1,3-diazadihydroazulanone

Chemical Property:

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Technology Process of 1-p-chlorophenyl-6-tosyl-1,3-diazadihydroazulanone

There total 2 articles about 1-p-chlorophenyl-6-tosyl-1,3-diazadihydroazulanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

1-p-chlorophenyl-3-tosyldihydro-1,3-diazaazulanone (144104-62-1) → 1-p-chlorophenyl-6-tosyl-1,3-diazadihydroazulanone (262296-54-8)

Guidance literature:

With tetrabutylammonium perchlorate; In acetonitrile; at 0 ℃; Electrochemical reaction;

DOI:10.3987/COM-99-8749

Reference yield: 51.0%

1-p-chlorophenyl-3-tosyldihydro-1,3-diazaazulanone (144104-62-1) → 1-p-chlorophenyl-6-tosyl-1,3-diazadihydroazulanone (262296-54-8) + 1-(4-chloro-phenyl)-3-(toluene-4-sulfonyl)-3,6-dihydro-1H-cycloheptaimidazol-2-one

Guidance literature:

With tetrabutylammonium perchlorate; In acetonitrile; at 25 ℃; Electrochemical reaction;

DOI:10.3987/COM-02-S(M)19

Reference yield: 32.0%

1-p-chlorophenyl-6-tosyl-1,3-diazadihydroazulanone (262296-54-8) → N-(p-chlorophenyl)-1,3-diazaazulene (144104-64-3)

Guidance literature:

In acetonitrile; at 20 ℃; for 3h; UV-irradiation;

DOI:10.3987/COM-01-9341

upstream raw materials:

1-p-chlorophenyl-3-tosyldihydro-1,3-diazaazulanone

Downstream raw materials:

N-(p-chlorophenyl)-1,3-diazaazulene

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