3-[(diphenylphosphanyl)borane]-1-(triphenyphosphonio)benzo[c]phospholide

Base Information

Chemical Name:3-[(diphenylphosphanyl)borane]-1-(triphenyphosphonio)benzo[c]phospholide
CAS No.:455947-56-5
Molecular Formula:C₃₈H₂₉P₃S
Molecular Weight:610.636
Hs Code.:

Synonyms:3-[(diphenylphosphanyl)borane]-1-(triphenyphosphonio)benzo[c]phospholide

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Chemical Property of 3-[(diphenylphosphanyl)borane]-1-(triphenyphosphonio)benzo[c]phospholide

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Technology Process of 3-[(diphenylphosphanyl)borane]-1-(triphenyphosphonio)benzo[c]phospholide

There total 3 articles about 3-[(diphenylphosphanyl)borane]-1-(triphenyphosphonio)benzo[c]phospholide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 235754-80-0
3-(diphenylphosphanyl)-1-(triphenyphosphonio)benzo[c]phospholide

: 455947-56-5
3-[(diphenylphosphanyl)borane]-1-(triphenyphosphonio)benzo[c]phospholide

Guidance literature:: With sulfur; In tetrahydrofuran; for 12h;

Reference yield:

: 1,3-bis(triphenylphosphonio)benzo[c]phospholide chloride

: 455947-56-5
3-[(diphenylphosphanyl)borane]-1-(triphenyphosphonio)benzo[c]phospholide

Guidance literature:: Multi-step reaction with 2 steps

1: 47 percent / [Mg(thf)3(C₁₄H₁₀)] / tetrahydrofuran / 8 h

2: 87 percent / S₈ / tetrahydrofuran / 12 h

With sulfur; [Mg(thf)3(C₁₄H₁₀)]; In tetrahydrofuran;

Reference yield:

: 10544-50-0
sulfur

: [tricarbonyl-η5-(3-diphenylphosphinyl-1-triphenylphosphoniobenzo[c]phospholide)chromium(0)]*pentane

: 479199-97-8
[tetracarbonyl-(1-triphenylphosphonio-3-diphenylthioxophosphoranylbenzo[c]phospholide-κ2-P,S)chromium(0)]*THF

: 455947-56-5
3-[(diphenylphosphanyl)borane]-1-(triphenyphosphonio)benzo[c]phospholide

Guidance literature:: In tetrahydrofuran; (Ar); dissolving of Cr(CO)3(C6H4C(PPh3)PC(PPh2)) in THF; addn. of equimolar amt. of solid S8; monitoring by NMR;
DOI:10.1021/om020404v