Technology Process of C39H49N7O5S2
There total 5 articles about C39H49N7O5S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
acetic acid;
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
N,N-dimethyl-formamide;
for 0.666667h;
C37H47N7O4S2;
With
triethylamine;
In
N,N-dimethyl-formamide;
for 3h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride / 1,4-dioxane; methanol
2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1.33 h / Inert atmosphere; Cooling with ice
2.2: 16 h / 20 °C
3.1: sodium hydroxide / water; methanol / 16 h / pH 13
4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.67 h
4.2: 3 h
With
hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydroxide; water / ethanol / 3 h
1.2: pH 9
1.3: 16 h / 45 °C
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h
2.2: 2 h
3.1: hydrogenchloride / 1,4-dioxane; methanol
4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1.33 h / Inert atmosphere; Cooling with ice
4.2: 16 h / 20 °C
5.1: sodium hydroxide / water; methanol / 16 h / pH 13
6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.67 h
6.2: 3 h
With
hydrogenchloride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;