2S-(2β,3β,4α,5α) 4-azido-5-hydroxy-2,3-bis<(4-methoxyphenyl)methoxy>-cyclohexanone

Base Information

Chemical Name:2S-(2β,3β,4α,5α) 4-azido-5-hydroxy-2,3-bis<(4-methoxyphenyl)methoxy>-cyclohexanone
CAS No.:153165-81-2
Molecular Formula:C₂₂H₂₅N₃O₆
Molecular Weight:427.457
Hs Code.:

Synonyms:2S-(2β,3β,4α,5α) 4-azido-5-hydroxy-2,3-bis<(4-methoxyphenyl)methoxy>-cyclohexanone

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Chemical Property of 2S-(2β,3β,4α,5α) 4-azido-5-hydroxy-2,3-bis<(4-methoxyphenyl)methoxy>-cyclohexanone

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Technology Process of 2S-(2β,3β,4α,5α) 4-azido-5-hydroxy-2,3-bis<(4-methoxyphenyl)methoxy>-cyclohexanone

There total 5 articles about 2S-(2β,3β,4α,5α) 4-azido-5-hydroxy-2,3-bis<(4-methoxyphenyl)methoxy>-cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: methyl 2-azido-2,6-dideoxy-3,4-di-O-<(4-methoxyphenyl)methyl>-α-D-arabino-hex-5-enopyranoside

: 153165-81-2
2S-(2β,3β,4α,5α) 4-azido-5-hydroxy-2,3-bis<(4-methoxyphenyl)methoxy>-cyclohexanone

Guidance literature:: With Hg(II) trifluoroacetate; In water; acetone; at 20 ℃;
DOI:10.1016/S0040-4020(01)87223-9

Reference yield:

: 116003-77-1
2-azido-2-deoxy-4,6-O-(phenylmethylene)methyl-α-D-altropyranoside

: 153165-81-2
2S-(2β,3β,4α,5α) 4-azido-5-hydroxy-2,3-bis<(4-methoxyphenyl)methoxy>-cyclohexanone

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / NBS, CaCO₃ / CCl₄ / 80 °C

2: MeONa / methanol

3: NaH / dimethylformamide

4: 74 percent / Hg(CF₃CO₂)2 / acetone; H₂O / 20 °C

With N-Bromosuccinimide; Hg(II) trifluoroacetate; sodium methylate; sodium hydride; calcium carbonate; In methanol; tetrachloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4020(01)87223-9

Reference yield:

: 2746-25-0
p-Methoxybenzyl bromide

: 153165-81-2
2S-(2β,3β,4α,5α) 4-azido-5-hydroxy-2,3-bis<(4-methoxyphenyl)methoxy>-cyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / dimethylformamide

2: 74 percent / Hg(CF₃CO₂)2 / acetone; H₂O / 20 °C

With Hg(II) trifluoroacetate; sodium hydride; In water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4020(01)87223-9