(E)-3-(2-((2,6-diphenyl-4H-pyran-4-ylidene)methyl)thiazol-5-yl)acrylaldehyde

Base Information

Chemical Name:(E)-3-(2-((2,6-diphenyl-4H-pyran-4-ylidene)methyl)thiazol-5-yl)acrylaldehyde
CAS No.:1388020-64-1
Molecular Formula:C₂₄H₁₇NO₂S
Molecular Weight:383.47
Hs Code.:

Synonyms:(E)-3-(2-((2,6-diphenyl-4H-pyran-4-ylidene)methyl)thiazol-5-yl)acrylaldehyde

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Chemical Property of (E)-3-(2-((2,6-diphenyl-4H-pyran-4-ylidene)methyl)thiazol-5-yl)acrylaldehyde

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Technology Process of (E)-3-(2-((2,6-diphenyl-4H-pyran-4-ylidene)methyl)thiazol-5-yl)acrylaldehyde

There total 1 articles about (E)-3-(2-((2,6-diphenyl-4H-pyran-4-ylidene)methyl)thiazol-5-yl)acrylaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 129806-51-5
2,6-diphenyl-(4H-pyran-4ylidene)-diphenylphosphine oxide

: 1388020-64-1
(E)-3-(2-((2,6-diphenyl-4H-pyran-4-ylidene)methyl)thiazol-5-yl)acrylaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

2.2: -78 - 0 °C / Inert atmosphere

With n-butyllithium; In tetrahydrofuran; hexane; 1.1: Horner-Wadsworth-Emmons olefination / 1.2: Horner-Wadsworth-Emmons olefination;
DOI:10.1016/j.tet.2012.05.123