Technology Process of C29H32N2O7
There total 6 articles about C29H32N2O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 0 - 25 ℃;
for 2h;
DOI:10.1021/ja500548e
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap
2: 1,2-dichloro-benzene / 230 °C
3: acetic acid; sodium cyanoborohydride / isopropyl alcohol / 16 h / 25 °C
4: hydrogen
5: ChiralCel OD column / isopropyl alcohol; hexane / Resolution of racemate
6: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 25 °C
With
dmap; tetrabutyl ammonium fluoride; hydrogen; sodium cyanoborohydride; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; hexane; 1,2-dichloro-benzene; isopropyl alcohol;
DOI:10.1021/ja500548e
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1,2-dichloro-benzene / 230 °C
2: acetic acid; sodium cyanoborohydride / isopropyl alcohol / 16 h / 25 °C
3: hydrogen
4: ChiralCel OD column / isopropyl alcohol; hexane / Resolution of racemate
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 25 °C
With
tetrabutyl ammonium fluoride; hydrogen; sodium cyanoborohydride; acetic acid;
In
tetrahydrofuran; hexane; 1,2-dichloro-benzene; isopropyl alcohol;
DOI:10.1021/ja500548e
