Alpha-isopropyl-alpha-[3-[N-[2-(2-methoxyphenoxy)ethyl]amino]propyl]-3,4,5-trimethoxyphenylacetonitrile

Base Information

Chemical Name:Alpha-isopropyl-alpha-[3-[N-[2-(2-methoxyphenoxy)ethyl]amino]propyl]-3,4,5-trimethoxyphenylacetonitrile
CAS No.:103524-24-9
Molecular Formula:C₂₆H₃₆N₂O₅
Molecular Weight:456.582
Hs Code.:

Synonyms:Alpha-isopropyl-alpha-[3-[N-[2-(2-methoxyphenoxy)ethyl]amino]propyl]-3,4,5-trimethoxyphenylacetonitrile

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Chemical Property of Alpha-isopropyl-alpha-[3-[N-[2-(2-methoxyphenoxy)ethyl]amino]propyl]-3,4,5-trimethoxyphenylacetonitrile

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Technology Process of Alpha-isopropyl-alpha-[3-[N-[2-(2-methoxyphenoxy)ethyl]amino]propyl]-3,4,5-trimethoxyphenylacetonitrile

There total 4 articles about Alpha-isopropyl-alpha-[3-[N-[2-(2-methoxyphenoxy)ethyl]amino]propyl]-3,4,5-trimethoxyphenylacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36622-33-0
α-isopropyl-3,4,5-trimethoxybenzenacetonitrilie

: 103524-24-9
Alpha-isopropyl-alpha-[3-[N-[2-(2-methoxyphenoxy)ethyl]amino]propyl]-3,4,5-trimethoxyphenylacetonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 180.45 g / NaNH₂ / tetrahydrofuran / 3.5 h / Heating

2: 91 percent / (COOH)2*2H₂O / acetone; H₂O / 1.5 h / Heating

3: 2.) NaBH₄ / 1.) MeOH, 1 H, reflux, 2.) MeOH, ice water, 1 h, room temp.

With sodium tetrahydroborate; oxalic acid; sodium amide; In tetrahydrofuran; water; acetone;
DOI:10.1248/cpb.36.367

Reference yield:

: 66332-85-2
α-(3,3-diethoxypropyl)-α-isopropyl-3,4,5-trimethoxybenzeneacetonitrile

: 103524-24-9
Alpha-isopropyl-alpha-[3-[N-[2-(2-methoxyphenoxy)ethyl]amino]propyl]-3,4,5-trimethoxyphenylacetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / (COOH)2*2H₂O / acetone; H₂O / 1.5 h / Heating

2: 2.) NaBH₄ / 1.) MeOH, 1 H, reflux, 2.) MeOH, ice water, 1 h, room temp.

With sodium tetrahydroborate; oxalic acid; In water; acetone;
DOI:10.1248/cpb.36.367

Reference yield:

: 1836-62-0
2-(2-methoxy-phenoxy)-ethylamine

: 66332-86-3
α-(2-formylethyl)-α-isopropyl-3,4,5-trimethoxybenzeneacetonitrile

: 103524-24-9
Alpha-isopropyl-alpha-[3-[N-[2-(2-methoxyphenoxy)ethyl]amino]propyl]-3,4,5-trimethoxyphenylacetonitrile

Guidance literature:: With sodium tetrahydroborate; Yield given. Multistep reaction; 1.) MeOH, 1 H, reflux, 2.) MeOH, ice water, 1 h, room temp.;
DOI:10.1248/cpb.36.367