(S)-2-((1S,2S)-2-tert-Butoxycarbonylamino-1-carbamoyl-3-phenyl-propylamino)-4-methyl-pentanoic acid methyl ester

Base Information

• Chemical Name: (S)-2-((1S,2S)-2-tert-Butoxycarbonylamino-1-carbamoyl-3-phenyl-propylamino)-4-methyl-pentanoic acid methyl ester
• CAS No.: 158999-87-2
• Molecular Formula: C₂₂H₃₅N₃O₅
• Molecular Weight: 421.537

Synonyms:(S)-2-((1S,2S)-2-tert-Butoxycarbonylamino-1-carbamoyl-3-phenyl-propylamino)-4-methyl-pentanoic acid methyl ester

Chemical Property of (S)-2-((1S,2S)-2-tert-Butoxycarbonylamino-1-carbamoyl-3-phenyl-propylamino)-4-methyl-pentanoic acid methyl ester

Chemical Property:

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Technology Process of (S)-2-((1S,2S)-2-tert-Butoxycarbonylamino-1-carbamoyl-3-phenyl-propylamino)-4-methyl-pentanoic acid methyl ester

There total 1 articles about (S)-2-((1S,2S)-2-tert-Butoxycarbonylamino-1-carbamoyl-3-phenyl-propylamino)-4-methyl-pentanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

Boc-PheψLeu-OMe (431063-61-5) → (S)-2-((1S,2S)-2-tert-Butoxycarbonylamino-1-carbamoyl-3-phenyl-propylamino)-4-methyl-pentanoic acid methyl ester (158999-87-2) + (1'S,3S,5S)-3-<1'-<(tert-Butyloxycarbonyl)amino>-2'-phenylethyl>-5-isobutyl-2,6-dioxopiperazine + (1'S,3R,5S)-3-<1'-<(tert-Butyloxycarbonyl)amino>-2'-phenylethyl>-5-isobutyl-2,6-dioxopiperazine

Guidance literature:

With sodium hydroxide; dihydrogen peroxide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; at 0 ℃; for 4h;

DOI:10.1021/jo00092a019

Reference yield:

(S)-2-((1S,2S)-2-tert-Butoxycarbonylamino-1-carbamoyl-3-phenyl-propylamino)-4-methyl-pentanoic acid methyl ester (158999-87-2) → (1'S,3S,5S)-3-<1'-<(tert-Butyloxycarbonyl)amino>-2'-phenylethyl>-5-isobutyl-2,6-dioxopiperazine

Guidance literature:

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; for 1h; Yield given;

DOI:10.1021/jo00092a019

Reference yield:

(S)-2-((1S,2S)-2-tert-Butoxycarbonylamino-1-carbamoyl-3-phenyl-propylamino)-4-methyl-pentanoic acid methyl ester (158999-87-2) → (S)-2-((1S,2S)-2-Amino-1-carbamoyl-3-phenyl-propylamino)-4-methyl-pentanoic acid methyl ester

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 4h; Ambient temperature;

DOI:10.1021/jo00092a019

upstream raw materials:

Boc-PheψLeu-OMe

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