6-Benzenesulfinyl-2,2-di-tert-butyl-4,5,7,8-tetramethyl-4H-benzo[1,3,2]dioxasiline

Base Information

Chemical Name:6-Benzenesulfinyl-2,2-di-tert-butyl-4,5,7,8-tetramethyl-4H-benzo[1,3,2]dioxasiline
CAS No.:183199-43-1
Molecular Formula:C₂₅H₃₆O₃SSi
Molecular Weight:444.711
Hs Code.:

Synonyms:6-Benzenesulfinyl-2,2-di-tert-butyl-4,5,7,8-tetramethyl-4H-benzo[1,3,2]dioxasiline

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Chemical Property of 6-Benzenesulfinyl-2,2-di-tert-butyl-4,5,7,8-tetramethyl-4H-benzo[1,3,2]dioxasiline

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Technology Process of 6-Benzenesulfinyl-2,2-di-tert-butyl-4,5,7,8-tetramethyl-4H-benzo[1,3,2]dioxasiline

There total 3 articles about 6-Benzenesulfinyl-2,2-di-tert-butyl-4,5,7,8-tetramethyl-4H-benzo[1,3,2]dioxasiline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2,2-Di-tert-butyl-4,5,7,8-tetramethyl-6-phenylsulfanyl-4H-benzo[1,3,2]dioxasiline

: 183199-43-1
6-Benzenesulfinyl-2,2-di-tert-butyl-4,5,7,8-tetramethyl-4H-benzo[1,3,2]dioxasiline

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -30 ℃; Yield given;
DOI:10.1016/0040-4039(96)01713-3

Reference yield:

: 85272-31-7
di-tert-butylsilyl bis(trifluoromethanesulfonate)

: 183199-43-1
6-Benzenesulfinyl-2,2-di-tert-butyl-4,5,7,8-tetramethyl-4H-benzo[1,3,2]dioxasiline

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂

2: mCPBA

With pyridine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1080/10426509708545516

Reference yield:

: 2-(1-Hydroxy-ethyl)-3,5,6-trimethyl-4-phenylsulfanyl-phenol

: 183199-43-1
6-Benzenesulfinyl-2,2-di-tert-butyl-4,5,7,8-tetramethyl-4H-benzo[1,3,2]dioxasiline

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂

2: mCPBA

With pyridine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1080/10426509708545516