tris(trans-1,2-cyclopropanediyldimethylene) diborate

Base Information

Chemical Name:tris(trans-1,2-cyclopropanediyldimethylene) diborate
CAS No.:86022-60-8
Molecular Formula:C₁₅H₂₄B₂O₆
Molecular Weight:321.974
Hs Code.:

Synonyms:tris(trans-1,2-cyclopropanediyldimethylene) diborate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tris(trans-1,2-cyclopropanediyldimethylene) diborate

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Technology Process of tris(trans-1,2-cyclopropanediyldimethylene) diborate

There total 1 articles about tris(trans-1,2-cyclopropanediyldimethylene) diborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 58616-95-8
trans-1,2-cyclopropanedicarboxylic acid

: 13283-31-3
borane

: 86022-60-8
tris(trans-1,2-cyclopropanediyldimethylene) diborate

: 11113-50-1,14635-83-7
boric acid

Guidance literature:: In tetrahydrofuran; byproducts: trans-1,2-bis(hydroxymethyl)cyclopropane; trans-1,2-cyclopropanedicarboxylic acid soln. added dropwise to cooled,stirred BH3 soln., stirred for 3 h at room temp.; cooled (ice bath), ice slowly added, THF evapd. (vac.), dil. acid or base added, stirred at 60°C for 3 h, extd. (ether), extd. (CHCl3), recrystd. (CHCl3); elem. anal.;