Technology Process of C16H18O2
There total 4 articles about C16H18O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydroxide; lithium aluminium tetrahydride;
In
diethyl ether; water;
for 0.75h;
Ice cooling;
Heating / reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.17 h / -78 °C / Argon atmosphere
1.2: 0.75 h / Ice cooling
2.1: hydrogenchloride; hydrogen / 10% palladium on activated carbon / methanol / 18 h / 20 °C
3.1: sodium hydroxide; lithium aluminium tetrahydride / diethyl ether; water / 0.75 h / Ice cooling; Heating / reflux
With
hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; hydrogen; tert.-butyl lithium;
10% palladium on activated carbon;
In
tetrahydrofuran; methanol; diethyl ether; water; pentane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride; hydrogen / 10% palladium on activated carbon / methanol / 18 h / 20 °C
2: sodium hydroxide; lithium aluminium tetrahydride / diethyl ether; water / 0.75 h / Ice cooling; Heating / reflux
With
hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; hydrogen;
10% palladium on activated carbon;
In
methanol; diethyl ether; water;