methyl 3-(N-(2-morpholinoethyl)methylsulfonamido)-4-(trifluoromethoxy)benzoate

Base Information

Chemical Name:methyl 3-(N-(2-morpholinoethyl)methylsulfonamido)-4-(trifluoromethoxy)benzoate
CAS No.:1610862-18-4
Molecular Formula:C₁₆H₂₁F₃N₂O₆S
Molecular Weight:426.414
Hs Code.:

Synonyms:methyl 3-(N-(2-morpholinoethyl)methylsulfonamido)-4-(trifluoromethoxy)benzoate

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Chemical Property of methyl 3-(N-(2-morpholinoethyl)methylsulfonamido)-4-(trifluoromethoxy)benzoate

Chemical Property:

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Technology Process of methyl 3-(N-(2-morpholinoethyl)methylsulfonamido)-4-(trifluoromethoxy)benzoate

There total 5 articles about methyl 3-(N-(2-morpholinoethyl)methylsulfonamido)-4-(trifluoromethoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀H₁₀F₃NO₅S

: 3647-69-6
4-(2-chloroethyl)morpholine hydrochride

: 1610862-18-4
methyl 3-(N-(2-morpholinoethyl)methylsulfonamido)-4-(trifluoromethoxy)benzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃;

Reference yield:

: 784-77-0
3-nitro-4-(trifluoromethoxy)benzoic acid

: 1610862-18-4
methyl 3-(N-(2-morpholinoethyl)methylsulfonamido)-4-(trifluoromethoxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / Reflux

2: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 1034.32 Torr

3: pyridine / 0 - 20 °C

4: potassium carbonate / N,N-dimethyl-formamide / 100 °C

With pyridine; sulfuric acid; palladium 10% on activated carbon; hydrogen; potassium carbonate; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 330-12-1
4-trifluoromethoxybenzoic acid

: 1610862-18-4
methyl 3-(N-(2-morpholinoethyl)methylsulfonamido)-4-(trifluoromethoxy)benzoate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium nitrate; sulfuric acid / 2 h / 0 °C

2: sulfuric acid / Reflux

3: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 1034.32 Torr

4: pyridine / 0 - 20 °C

5: potassium carbonate / N,N-dimethyl-formamide / 100 °C

With pyridine; sulfuric acid; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium nitrate; In methanol; N,N-dimethyl-formamide;