trimethyl 2,6-dimethyl-4-(2-<2-(1,3-dioxolanyl)>phenyl)-1,4-dihydropyridine-1,3,5-tricarboxylate

Base Information

• Chemical Name: trimethyl 2,6-dimethyl-4-(2-<2-(1,3-dioxolanyl)>phenyl)-1,4-dihydropyridine-1,3,5-tricarboxylate
• CAS No.: 98014-99-4
• Molecular Formula: C₂₂H₂₅NO₈
• Molecular Weight: 431.442

Synonyms:trimethyl 2,6-dimethyl-4-(2-<2-(1,3-dioxolanyl)>phenyl)-1,4-dihydropyridine-1,3,5-tricarboxylate

Chemical Property of trimethyl 2,6-dimethyl-4-(2-<2-(1,3-dioxolanyl)>phenyl)-1,4-dihydropyridine-1,3,5-tricarboxylate

Chemical Property:

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Technology Process of trimethyl 2,6-dimethyl-4-(2-<2-(1,3-dioxolanyl)>phenyl)-1,4-dihydropyridine-1,3,5-tricarboxylate

There total 1 articles about trimethyl 2,6-dimethyl-4-(2-<2-(1,3-dioxolanyl)>phenyl)-1,4-dihydropyridine-1,3,5-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyl 2,6-dimethyl-4-<2-(2-(1,3-dioxolanyl))phenyl>-1,4-dihydropyridine-3,5-dicarboxylate (96557-29-8) + methyl chloroformate (79-22-1) → trimethyl 2,6-dimethyl-4-(2-<2-(1,3-dioxolanyl)>phenyl)-1,4-dihydropyridine-1,3,5-tricarboxylate (98014-99-4)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) THF, DMF, reflux, 15 min, 2.) THF, DMF, reflux, 18 h;

DOI:10.1021/jo00221a030

Reference yield: 49.0%

trimethyl 2,6-dimethyl-4-(2-<2-(1,3-dioxolanyl)>phenyl)-1,4-dihydropyridine-1,3,5-tricarboxylate (98014-99-4) → 4-(2-Formyl-phenyl)-2,6-dimethyl-4H-pyridine-1,3,5-tricarboxylic acid trimethyl ester (98015-00-0)

Guidance literature:

With toluene-4-sulfonic acid; In acetone; for 2.5h; Ambient temperature;

DOI:10.1021/jo00221a030

upstream raw materials:

dimethyl 2,6-dimethyl-4-<2-(2-(1,3-dioxolanyl))phenyl>-1,4-dihydropyridine-3,5-dicarboxylate

methyl chloroformate

Downstream raw materials:

4-(2-Formyl-phenyl)-2,6-dimethyl-4H-pyridine-1,3,5-tricarboxylic acid trimethyl ester

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