4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester

Base Information

Chemical Name:4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester
CAS No.:1437306-59-6
Molecular Formula:C₁₉H₂₉N₃O₈
Molecular Weight:427.455
Hs Code.:

Synonyms:4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester

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Chemical Property of 4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester

Chemical Property:

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Technology Process of 4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester

There total 1 articles about 4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 530-57-4
3,5-dimethoxy-4-hydroxybenzoic acid

: 1437306-59-6
4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 0 - 20 °C

2: caesium carbonate / N,N-dimethyl-formamide / 4 h / 70 °C

With thionyl chloride; caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/bc400074w

Reference yield: 99.0%

: 1437306-59-6
4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester

: 1437306-81-4
4-(2-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester

Guidance literature:: With hydrogen; palladium diacetate; In ethanol;
DOI:10.1021/bc400074w

Reference yield:

: 1437306-59-6
4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester

: 1437306-78-9
C₃₂H₄₂N₄O₁₂*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 6 steps

1: palladium diacetate; hydrogen / ethanol

2: methanol; tert-butyl alcohol / 20 °C

3: lithium hydroxide / tetrahydrofuran; methanol; water / 20 °C

4: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; TBTU / N,N-dimethyl-formamide; water / 0 - 20 °C

5: potassium hydroxide; hydroxylamine hydrochloride / methanol / 24 h / 20 °C / Inert atmosphere

6: dichloromethane / 24 h / 20 °C

With TBTU; hydroxylamine hydrochloride; hydrogen; palladium diacetate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; potassium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/bc400074w