6-chloro-6-deoxyascorbic acid

Base Information

Chemical Name:6-chloro-6-deoxyascorbic acid
CAS No.:62983-43-1
Molecular Formula:C6H7ClO5
Molecular Weight:194.57
Hs Code.:

Synonyms:(R)-5-((R)-2-Chloro-1-hydroxy-ethyl)-3,4-dihydroxy-5H-furan-2-one;

Suppliers and Price of 6-chloro-6-deoxyascorbic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-chloro-6-deoxyascorbic acid

Chemical Property:

Vapor Pressure:1.18E-06mmHg at 25°C
Melting Point:147 - 149 °C
Boiling Point:360.6°C at 760 mmHg
PKA:3.99±0.10(Predicted)
Flash Point:171.9°C
PSA：86.99000
Density:1.87g/cm³
LogP:-0.16090

Purity/Quality:

Safty Information:

Pictogram(s):
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Technology Process of 6-chloro-6-deoxyascorbic acid

There total 5 articles about 6-chloro-6-deoxyascorbic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 50-81-7,98966-42-8
ascorbic acid

: 62983-43-1
6-Desoxy-6-chlor-L-ascorbinsaeure

Guidance literature:: With hydrogenchloride; In formic acid; at 50 ℃; under 294.2 - 441.3 Torr;
DOI:10.1002/hlca.19800630642

Reference yield:

: 18467-77-1
dikegulac

: 62983-43-1
6-Desoxy-6-chlor-L-ascorbinsaeure

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / K₂CO₃ / dimethylformamide / 4 h / Ambient temperature

2: 13 g / Cu(Ac)2 / H₂O / 0.08 h

3: 64.5 percent / CCl₄, PPh₃ / various solvent(s) / 0.08 h / Heating

4: Amberlite JR 120 (H+-form), H₂O / 4 h / Heating

With tetrachloromethane; Amberlite JR 120 (H+-form); water; copper diacetate; potassium carbonate; triphenylphosphine; In water; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19800630642

Reference yield:

: 52507-90-1
methyl 2,3:4,6-di-O-isopropylidene-α-L-xylo-2-hexulofuranosonate

: 62983-43-1
6-Desoxy-6-chlor-L-ascorbinsaeure

Guidance literature:: Multi-step reaction with 3 steps

1: 13 g / Cu(Ac)2 / H₂O / 0.08 h

2: 64.5 percent / CCl₄, PPh₃ / various solvent(s) / 0.08 h / Heating

3: Amberlite JR 120 (H+-form), H₂O / 4 h / Heating

With tetrachloromethane; Amberlite JR 120 (H+-form); water; copper diacetate; triphenylphosphine; In water;
DOI:10.1002/hlca.19800630642