(+/-)-celallocinnine

Base Information

Chemical Name:(+/-)-celallocinnine
CAS No.:79435-40-8
Molecular Formula:C₂₅H₃₁N₃O₂
Molecular Weight:405.54
Hs Code.:

Synonyms:(+/-)-celallocinnine

Suppliers and Price of (+/-)-celallocinnine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-celallocinnine

Chemical Property:

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Technology Process of (+/-)-celallocinnine

There total 7 articles about (+/-)-celallocinnine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 73465-24-4
(+/-)-celacinnine

: 79435-40-8
(+/-)-celallocinnine

Guidance literature:: In benzene; for 35h; Irradiation;
DOI:10.1021/ja00410a025

Reference yield:

: 4748-73-6
N-(cyanoethyl)-1,4-diaminobutane

: 79435-40-8
(+/-)-celallocinnine

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / ethanol / 2 h / Heating

2: 81 percent / H₂ / PtO₂ / CHCl₃; ethanol / 8 h / 25 °C / 760 Torr

3: 90 percent / B(NMe₂)3 / xylene / 0.5 h / 25 °C

4: 97 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 1.) -78 deg C, 2.5 h, 2.) -20 deg C, 10 h

5: 50 percent / benzene / 35 h / Irradiation

With dmap; tris(dimethylamino)borane; hydrogen; platinum(IV) oxide; In ethanol; dichloromethane; chloroform; xylene; benzene;
DOI:10.1021/ja00410a025

Reference yield:

: 79405-59-7
ethyl 11-cyano-4,9-diaza-3-phenyl-2-undecenoate

: 79435-40-8
(+/-)-celallocinnine

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / H₂ / PtO₂ / CHCl₃; ethanol / 8 h / 25 °C / 760 Torr

2: 90 percent / B(NMe₂)3 / xylene / 0.5 h / 25 °C

3: 97 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 1.) -78 deg C, 2.5 h, 2.) -20 deg C, 10 h

4: 50 percent / benzene / 35 h / Irradiation

With dmap; tris(dimethylamino)borane; hydrogen; platinum(IV) oxide; In ethanol; dichloromethane; chloroform; xylene; benzene;
DOI:10.1021/ja00410a025