ethyl P-(4-bromo-1,3-bis[(dimethylamino)methyl]phenyl)-N,N-dimethylaminophosphinate

Base Information

Chemical Name:ethyl P-(4-bromo-1,3-bis[(dimethylamino)methyl]phenyl)-N,N-dimethylaminophosphinate
CAS No.:1186435-33-5
Molecular Formula:C₁₆H₂₉BrN₃O₂P
Molecular Weight:406.303
Hs Code.:

Synonyms:ethyl P-(4-bromo-1,3-bis[(dimethylamino)methyl]phenyl)-N,N-dimethylaminophosphinate

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Chemical Property of ethyl P-(4-bromo-1,3-bis[(dimethylamino)methyl]phenyl)-N,N-dimethylaminophosphinate

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Technology Process of ethyl P-(4-bromo-1,3-bis[(dimethylamino)methyl]phenyl)-N,N-dimethylaminophosphinate

There total 1 articles about ethyl P-(4-bromo-1,3-bis[(dimethylamino)methyl]phenyl)-N,N-dimethylaminophosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 2510-93-2
ethyl N,N-dimethylphosphoroamidochloridate

: 312304-54-4
1-bromo-4-iodo-2,6-bis[(dimethylamino)methyl]benzene

: 1186435-33-5
ethyl P-(4-bromo-1,3-bis[(dimethylamino)methyl]phenyl)-N,N-dimethylaminophosphinate

Guidance literature:: 1-bromo-4-iodo-2,6-bis[(dimethylamino)methyl]benzene; With tert.-butyl lithium; In diethyl ether; pentane; at -100 ℃; Inert atmosphere;

ethyl N,N-dimethylphosphoroamidochloridate; In diethyl ether; pentane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejic.200800654