5-[3,5-dichloro-4-(phosphonoxy)benzylidene]-3-(4-methoxyphenyl)-2-thioxo-1,3-oxazolidin-4-one

Base Information

Chemical Name:5-[3,5-dichloro-4-(phosphonoxy)benzylidene]-3-(4-methoxyphenyl)-2-thioxo-1,3-oxazolidin-4-one
CAS No.:1296646-53-1
Molecular Formula:C₁₇H₁₂Cl₂NO₇PS
Molecular Weight:476.231
Hs Code.:

Synonyms:5-[3,5-dichloro-4-(phosphonoxy)benzylidene]-3-(4-methoxyphenyl)-2-thioxo-1,3-oxazolidin-4-one

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Chemical Property of 5-[3,5-dichloro-4-(phosphonoxy)benzylidene]-3-(4-methoxyphenyl)-2-thioxo-1,3-oxazolidin-4-one

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Technology Process of 5-[3,5-dichloro-4-(phosphonoxy)benzylidene]-3-(4-methoxyphenyl)-2-thioxo-1,3-oxazolidin-4-one

There total 5 articles about 5-[3,5-dichloro-4-(phosphonoxy)benzylidene]-3-(4-methoxyphenyl)-2-thioxo-1,3-oxazolidin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1296646-51-9
5-[3,5-dichloro-4-(phosphonoxy)benzylidene]-3-(4-methoxyphenyl)-2-thioxo-1,3oxazolidin-4-one dibenzyl ester

: 1296646-53-1
5-[3,5-dichloro-4-(phosphonoxy)benzylidene]-3-(4-methoxyphenyl)-2-thioxo-1,3-oxazolidin-4-one

Guidance literature:: 5-[3,5-dichloro-4-(phosphonoxy)benzylidene]-3-(4-methoxyphenyl)-2-thioxo-1,3oxazolidin-4-one dibenzyl ester; With trimethylsilyl bromide; In chloroform; at 0 - 20 ℃; for 1.5h;

With hydrogenchloride; In chloroform; water; for 0.5h;
DOI:10.1016/j.bmc.2012.03.052

Reference yield:

: 1275574-75-8
5-(3,5-dichloro-4-hydroxybenzylidene)-3-(4-methoxyphenyl)-2-thioxo-1,3-oxazolidin-4-one

: 1296646-53-1
5-[3,5-dichloro-4-(phosphonoxy)benzylidene]-3-(4-methoxyphenyl)-2-thioxo-1,3-oxazolidin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; N-ethyl-N,N-diisopropylamine / tetrachloromethane / 1.5 h / -10 - 20 °C

2.1: trimethylsilyl bromide / chloroform / 1.5 h / 0 - 20 °C

2.2: 0.5 h

With dmap; trimethylsilyl bromide; N-ethyl-N,N-diisopropylamine; In tetrachloromethane; chloroform;
DOI:10.1016/j.bmc.2012.03.052

Reference yield:

: 2314-36-5
3,5-dichloro-4-hydroxybenzaldehyde

: 1296646-53-1
5-[3,5-dichloro-4-(phosphonoxy)benzylidene]-3-(4-methoxyphenyl)-2-thioxo-1,3-oxazolidin-4-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / 4 h / 120 °C

2.1: dmap; N-ethyl-N,N-diisopropylamine / tetrachloromethane / 1.5 h / -10 - 20 °C

3.1: trimethylsilyl bromide / chloroform / 1.5 h / 0 - 20 °C

3.2: 0.5 h

With dmap; trimethylsilyl bromide; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrachloromethane; chloroform; 1.1: Knoevenagel condensation;
DOI:10.1016/j.bmc.2012.03.052