meso-4,5-Diethyl-4,5-dimethyl-2-phenyl-4,5-dihydro-1H-imidazolyl-3-oxide-1-oxy

Base Information

Chemical Name:meso-4,5-Diethyl-4,5-dimethyl-2-phenyl-4,5-dihydro-1H-imidazolyl-3-oxide-1-oxy
CAS No.:351902-09-5
Molecular Formula:C₁₅H₂₁N₂O₂
Molecular Weight:261.344
Hs Code.:

Synonyms:meso-4,5-Diethyl-4,5-dimethyl-2-phenyl-4,5-dihydro-1H-imidazolyl-3-oxide-1-oxy

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Chemical Property of meso-4,5-Diethyl-4,5-dimethyl-2-phenyl-4,5-dihydro-1H-imidazolyl-3-oxide-1-oxy

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Technology Process of meso-4,5-Diethyl-4,5-dimethyl-2-phenyl-4,5-dihydro-1H-imidazolyl-3-oxide-1-oxy

There total 6 articles about meso-4,5-Diethyl-4,5-dimethyl-2-phenyl-4,5-dihydro-1H-imidazolyl-3-oxide-1-oxy which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 352004-79-6
(4R,5S)-4,5-Diethyl-4,5-dimethyl-2-phenyl-imidazolidine

: 351902-09-5
meso-4,5-Diethyl-4,5-dimethyl-2-phenyl-4,5-dihydro-1H-imidazolyl-3-oxide-1-oxy

: C₁₅H₂₁N₂O

Guidance literature:: (4R,5S)-4,5-Diethyl-4,5-dimethyl-2-phenyl-imidazolidine; With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 1h;

With sodium periodate; In dichloromethane; water; for 0.5h;
DOI:10.1002/ejoc.200400454

Reference yield:

: (2S,4R,5S)-4,5-Diethyl-4,5-dimethyl-2-phenyl-imidazolidine

: 351902-09-5
meso-4,5-Diethyl-4,5-dimethyl-2-phenyl-4,5-dihydro-1H-imidazolyl-3-oxide-1-oxy

Guidance literature:: With sodium hydroxide; In methanol; for 96h; Heating;
DOI:10.1021/ja0021060

Reference yield:

: 137946-64-6
meso-3,4-diamino-3,4-dimethylhexane

: 351902-09-5
meso-4,5-Diethyl-4,5-dimethyl-2-phenyl-4,5-dihydro-1H-imidazolyl-3-oxide-1-oxy

Guidance literature:: Multi-step reaction with 2 steps

1.1: 92 percent / diethyl ether

2.1: aq. NaHCO₃; m-chloroperbenzoic acid / CH₂Cl₂ / 1 h

2.2: 72 percent / NaIO₄ / CH₂Cl₂; H₂O / 0.5 h

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;
DOI:10.1002/ejoc.200400454