(E)-2-(2-(thiophen-2-yl)-2-p-tolylvinyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

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Chemical Name:(E)-2-(2-(thiophen-2-yl)-2-p-tolylvinyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine
CAS No.:1214265-08-3
Molecular Formula:C₂₃H₁₉BN₂S
Molecular Weight:366.294
Hs Code.:

Synonyms:(E)-2-(2-(thiophen-2-yl)-2-p-tolylvinyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

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Chemical Property of (E)-2-(2-(thiophen-2-yl)-2-p-tolylvinyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

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Technology Process of (E)-2-(2-(thiophen-2-yl)-2-p-tolylvinyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

There total 2 articles about (E)-2-(2-(thiophen-2-yl)-2-p-tolylvinyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 106-38-7
para-bromotoluene

: 1214264-94-4
(E)-ethyl 4-(2-(1H-naphtho[1,8-de][1,3,2]diazaborinin-2(3H)-yl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)benzoate

: 1214265-08-3
(E)-2-(2-(thiophen-2-yl)-2-p-tolylvinyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

Guidance literature:: With K₃PO₄; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; 80°C, 15 h;

Reference yield: 93.0%

: 106-38-7
para-bromotoluene

: 1214264-98-8
(E)-2-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-(thiophen-2-yl)vinyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

: 1214265-08-3
(E)-2-(2-(thiophen-2-yl)-2-p-tolylvinyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; In tetrahydrofuran; water; at 80 ℃; for 15h; chemoselective reaction;