3-(3,5-di-tert-butyl-2-hydroxyphenyl)-1-(2-(mesitylamino)phenyl)-4,5-dihydro-1H-imidazol-3-ium chloride

Base Information

Chemical Name:3-(3,5-di-tert-butyl-2-hydroxyphenyl)-1-(2-(mesitylamino)phenyl)-4,5-dihydro-1H-imidazol-3-ium chloride
CAS No.:1433417-13-0
Molecular Formula:C₃₂H₄₂N₃O*Cl
Molecular Weight:520.158
Hs Code.:

Synonyms:3-(3,5-di-tert-butyl-2-hydroxyphenyl)-1-(2-(mesitylamino)phenyl)-4,5-dihydro-1H-imidazol-3-ium chloride

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Chemical Property of 3-(3,5-di-tert-butyl-2-hydroxyphenyl)-1-(2-(mesitylamino)phenyl)-4,5-dihydro-1H-imidazol-3-ium chloride

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Technology Process of 3-(3,5-di-tert-butyl-2-hydroxyphenyl)-1-(2-(mesitylamino)phenyl)-4,5-dihydro-1H-imidazol-3-ium chloride

There total 4 articles about 3-(3,5-di-tert-butyl-2-hydroxyphenyl)-1-(2-(mesitylamino)phenyl)-4,5-dihydro-1H-imidazol-3-ium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1448426-16-1
N-(2-mesitylaminophenyl)-N'-(3,5-di-tert-butyl-2-hydroxyphenyl)-ethylenediamine

: 122-51-0
orthoformic acid triethyl ester

: 1433417-13-0
3-(3,5-di-tert-butyl-2-hydroxyphenyl)-1-(2-(mesitylamino)phenyl)-4,5-dihydro-1H-imidazol-3-ium chloride

Guidance literature:: N-(2-mesitylaminophenyl)-N'-(3,5-di-tert-butyl-2-hydroxyphenyl)-ethylenediamine; With hydrogenchloride; In methanol; water;

orthoformic acid triethyl ester; at 40 ℃; for 0.25h;
DOI:10.1039/c3sc22171g

Reference yield:

: 28448-17-1
N-(2’,4’,6’-trimethylphenyl)-1,2-phenylenediamine

: 1433417-13-0
3-(3,5-di-tert-butyl-2-hydroxyphenyl)-1-(2-(mesitylamino)phenyl)-4,5-dihydro-1H-imidazol-3-ium chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / tetrahydrofuran

2.1: triethylamine / toluene / Heating

3.1: lithium aluminium tetrahydride / tetrahydrofuran / Heating

4.1: hydrogenchloride / methanol; water

4.2: 0.25 h / 40 °C

With hydrogenchloride; lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; methanol; water; toluene;
DOI:10.1039/c3sc22171g

Reference yield:

: 1448426-14-9
C₁₉H₂₂N₂O₃

: 1433417-13-0
3-(3,5-di-tert-butyl-2-hydroxyphenyl)-1-(2-(mesitylamino)phenyl)-4,5-dihydro-1H-imidazol-3-ium chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / toluene / Heating

2.1: lithium aluminium tetrahydride / tetrahydrofuran / Heating

3.1: hydrogenchloride / methanol; water

3.2: 0.25 h / 40 °C

With hydrogenchloride; lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; methanol; water; toluene;
DOI:10.1039/c3sc22171g