5-hydroxymethyl-1-(methyl 2',3'-di-O-acetyl-5'-carbobenzyloxyamino-5'-deoxy-β-D-allofuranosyluronate)uracil

Base Information

Chemical Name:5-hydroxymethyl-1-(methyl 2',3'-di-O-acetyl-5'-carbobenzyloxyamino-5'-deoxy-β-D-allofuranosyluronate)uracil
CAS No.:310904-41-7
Molecular Formula:C₂₄H₂₇N₃O₁₂
Molecular Weight:549.491
Hs Code.:

Synonyms:5-hydroxymethyl-1-(methyl 2',3'-di-O-acetyl-5'-carbobenzyloxyamino-5'-deoxy-β-D-allofuranosyluronate)uracil

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Chemical Property of 5-hydroxymethyl-1-(methyl 2',3'-di-O-acetyl-5'-carbobenzyloxyamino-5'-deoxy-β-D-allofuranosyluronate)uracil

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Technology Process of 5-hydroxymethyl-1-(methyl 2',3'-di-O-acetyl-5'-carbobenzyloxyamino-5'-deoxy-β-D-allofuranosyluronate)uracil

There total 5 articles about 5-hydroxymethyl-1-(methyl 2',3'-di-O-acetyl-5'-carbobenzyloxyamino-5'-deoxy-β-D-allofuranosyluronate)uracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4433-40-3
5-hydroxymethyl uracil

: 310904-41-7
5-hydroxymethyl-1-(methyl 2',3'-di-O-acetyl-5'-carbobenzyloxyamino-5'-deoxy-β-D-allofuranosyluronate)uracil

Guidance literature:: Multi-step reaction with 4 steps

1: trimethylsilyl chloride / 12 h / Heating

2: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 1 h / Heating

3: H₂ / Pd-C / methanol / 20 °C

4: NaHCO₃ / toluene; dioxane / 1 h / 20 °C

With chloro-trimethyl-silane; trimethylsilyl trifluoromethanesulfonate; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In 1,4-dioxane; methanol; toluene; acetonitrile;

Reference yield:

: 127646-37-1
5-hydroxymethyl-1-(methyl 2',3'-di-O-acetyl-5'-azido-5'-deoxy-β-D-allofuranosyluronate)uracil

: 310904-41-7
5-hydroxymethyl-1-(methyl 2',3'-di-O-acetyl-5'-carbobenzyloxyamino-5'-deoxy-β-D-allofuranosyluronate)uracil

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd-C / methanol / 20 °C

2: NaHCO₃ / toluene; dioxane / 1 h / 20 °C

With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In 1,4-dioxane; methanol; toluene;

Reference yield:

: 155154-68-0
methyl (5-azido-5-deoxy-1,2,3-tri-O-acetyl-D-allofuranosid)uronate

: 310904-41-7
5-hydroxymethyl-1-(methyl 2',3'-di-O-acetyl-5'-carbobenzyloxyamino-5'-deoxy-β-D-allofuranosyluronate)uracil

Guidance literature:: Multi-step reaction with 3 steps

1: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 1 h / Heating

2: H₂ / Pd-C / methanol / 20 °C

3: NaHCO₃ / toluene; dioxane / 1 h / 20 °C

With trimethylsilyl trifluoromethanesulfonate; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In 1,4-dioxane; methanol; toluene; acetonitrile;